(PPh3)2Pd(η3-CH2C(N(i-Pr)2)CHPh)TOf

Base Information

• Chemical Name: (PPh3)2Pd(η3-CH2C(N(i-Pr)2)CHPh)TOf
• CAS No.: 539848-25-4
• Molecular Formula: C₇H₇O₃S*C₅₁H₅₂NP₂Pd
• Molecular Weight: 1018.54
• Mol file: 539848-25-4.mol

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Chemical Property of (PPh3)2Pd(η3-CH2C(N(i-Pr)2)CHPh)TOf

Chemical Property:

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Technology Process of (PPh3)2Pd(η3-CH2C(N(i-Pr)2)CHPh)TOf

There total 1 articles about (PPh3)2Pd(η3-CH2C(N(i-Pr)2)CHPh)TOf which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

[(PPh3)2Pd(η(3)-CH2CCPh)]OSO2C6H4CH3 (173539-36-1) + diisopropylamine (108-18-9) → (PPh3)2Pd(η3-CH2C(N(i-Pr)2)CHPh)TOf (539848-25-4)

Guidance literature:

In dichloromethane; amine was added to stirred soln. of Pd-complex in CH2Cl2 at room temp. under Ar, stirred for 10 min; solvent was removed under reduced pressure, washed with hexane, dried under vac. for several d;

DOI:10.1016/S0020-1693(02)01168-4

upstream raw materials:

[(PPh3)2Pd(η(3)-CH2CCPh)]OSO2C6H4CH3

diisopropylamine