(1,8-diphenylimino-3,6-dimethylcarbazolide)CoCl

Base Information

• Chemical Name: (1,8-diphenylimino-3,6-dimethylcarbazolide)CoCl
• CAS No.: 625385-48-0
• Molecular Formula: C₂₈H₂₂ClCoN₃
• Molecular Weight: 494.949
• Mol file: 625385-48-0.mol

Synonyms:

Chemical Property of (1,8-diphenylimino-3,6-dimethylcarbazolide)CoCl

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (1,8-diphenylimino-3,6-dimethylcarbazolide)CoCl

There total 1 articles about (1,8-diphenylimino-3,6-dimethylcarbazolide)CoCl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.0%

1,8-diphenylimino-3,6-dimethyl-9H-carbazole (625385-40-2) + cobalt(II) chloride (7646-79-9,14543-09-0,16413-89-1) → (1,8-diphenylimino-3,6-dimethylcarbazolide)CoCl (625385-48-0)

Guidance literature:

With NaH; In tetrahydrofuran; NaH and carbazole in THF were stirred at 65°C for 16 h, cooled toroom temp., filtered, added to a soln. CoCl2 in THF, stirred at room te mp. for 16 h (N2); the solvent was removed, extd. with CH2Cl2, concd., pptd. by addn. of pentane, filtered, washed with diethyl ether, dried in vac.; elem. anal.;

DOI:10.1039/b301902k

upstream raw materials:

1,8-diphenylimino-3,6-dimethyl-9H-carbazole

cobalt(II) chloride