Technology Process of C26H39NO3Si
There total 7 articles about C26H39NO3Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 7 steps
1: N,N,N',N'-tetramethyl-1,8-diaminonaphthalene / dichloromethane
2: palladium on activated charcoal; hydrogen / methanol
3: pyridine; hydrogen fluoride / tetrahydrofuran
4: di-isopropyl azodicarboxylate / tetrahydrofuran
5: diisobutylaluminium hydride / tetrahydrofuran / 0 °C
6: dmap; triethylamine
7: potassium carbonate; thiophenol / N,N-dimethyl-formamide
With
pyridine; dmap; di-isopropyl azodicarboxylate; palladium on activated charcoal; hydrogen fluoride; hydrogen; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; diisobutylaluminium hydride; potassium carbonate; thiophenol; triethylamine;
In
tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
4: Mitsunobu reaction;
DOI:10.1073/pnas.1015255108
- Guidance literature:
-
Multi-step reaction with 6 steps
1: palladium on activated charcoal; hydrogen / methanol
2: pyridine; hydrogen fluoride / tetrahydrofuran
3: di-isopropyl azodicarboxylate / tetrahydrofuran
4: diisobutylaluminium hydride / tetrahydrofuran / 0 °C
5: dmap; triethylamine
6: potassium carbonate; thiophenol / N,N-dimethyl-formamide
With
pyridine; dmap; di-isopropyl azodicarboxylate; palladium on activated charcoal; hydrogen fluoride; hydrogen; diisobutylaluminium hydride; potassium carbonate; thiophenol; triethylamine;
In
tetrahydrofuran; methanol; N,N-dimethyl-formamide;
3: Mitsunobu reaction;
DOI:10.1073/pnas.1015255108
- Guidance literature:
-
Multi-step reaction with 5 steps
1: pyridine; hydrogen fluoride / tetrahydrofuran
2: di-isopropyl azodicarboxylate / tetrahydrofuran
3: diisobutylaluminium hydride / tetrahydrofuran / 0 °C
4: dmap; triethylamine
5: potassium carbonate; thiophenol / N,N-dimethyl-formamide
With
pyridine; dmap; di-isopropyl azodicarboxylate; hydrogen fluoride; diisobutylaluminium hydride; potassium carbonate; thiophenol; triethylamine;
In
tetrahydrofuran; N,N-dimethyl-formamide;
2: Mitsunobu reaction;
DOI:10.1073/pnas.1015255108