tetraphenylporphyrin manganese(III) 4-bromophenylcyanamide

Base Information

• Chemical Name: tetraphenylporphyrin manganese(III) 4-bromophenylcyanamide
• CAS No.: 861641-03-4
• Molecular Formula: C₅₁H₃₂BrMnN₆
• Molecular Weight: 863.697
• Mol file: 861641-03-4.mol

Synonyms:

Chemical Property of tetraphenylporphyrin manganese(III) 4-bromophenylcyanamide

Chemical Property:

Purity/Quality:

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Technology Process of tetraphenylporphyrin manganese(III) 4-bromophenylcyanamide

There total 1 articles about tetraphenylporphyrin manganese(III) 4-bromophenylcyanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

(5,10,15,20-tetraphenylporphyrinato)manganese(III) chloride (34557-72-7,32195-55-4) + thallium(I) 4-bromophenylcyanamide → tetraphenylporphyrin manganese(III) 4-bromophenylcyanamide (861641-03-4)

Guidance literature:

In methanol; byproducts: TlCl; under N2, Schlenk setup, Mn compd. (0.11 mmol) and Tl compd. (0.59 mmol)mixed with methanol, stirred for 24 h; evapd., dissolved in CH2Cl2, filtered, concd., hexane added with stirring, pptd., filtered off, dried in air, elem. anal.;

DOI:10.1016/j.ica.2005.03.012

upstream raw materials:

(5,10,15,20-tetraphenylporphyrinato)manganese(III) chloride