di-iodo(σ-pentafluorophenyl)(p-tolylisocyanide)bis(triphenylphosphine)iridium

Base Information

• Chemical Name: di-iodo(σ-pentafluorophenyl)(p-tolylisocyanide)bis(triphenylphosphine)iridium
• CAS No.: 71817-55-5
• Molecular Formula: C₅₀H₃₇F₅I₂IrNP₂
• Molecular Weight: 1254.82
• Mol file: 71817-55-5.mol

Synonyms:

Chemical Property of di-iodo(σ-pentafluorophenyl)(p-tolylisocyanide)bis(triphenylphosphine)iridium

Chemical Property:

Purity/Quality:

Safty Information:

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Useful:

Technology Process of di-iodo(σ-pentafluorophenyl)(p-tolylisocyanide)bis(triphenylphosphine)iridium

There total 1 articles about di-iodo(σ-pentafluorophenyl)(p-tolylisocyanide)bis(triphenylphosphine)iridium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

Ir(C6F5)(CS)I2(P(C6H5)3)2 (71817-54-4) + p-toluidine (106-49-0,12221-03-3) → di-iodo(σ-pentafluorophenyl)(p-tolylisocyanide)bis(triphenylphosphine)iridium (71817-55-5)

Guidance literature:

In dichloromethane; N2-atmosphere; excess p-toluidine, gentle warming for 1 h, then room temp. for 20 h; concn. (evapn.), Et2O addn. (pptn.); elem. anal.;

DOI:10.1039/DT9790001053

upstream raw materials:

Ir(C₆F₅)(CS)I₂(P(C₆H₅)3)2

p-toluidine