C₃₀H₂₉N₅O₆

Base Information

• Chemical Name: C₃₀H₂₉N₅O₆
• CAS No.: 1373391-49-1
• Molecular Formula: C₃₀H₂₉N₅O₆
• Molecular Weight: 555.59
• Mol file: 1373391-49-1.mol

Synonyms:

Chemical Property of C₃₀H₂₉N₅O₆

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₀H₂₉N₅O₆

There total 6 articles about C₃₀H₂₉N₅O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

4'-azido-2'-deoxy-2'-methylarabinouridine (1158730-05-2) + mono-4-methoxytrityl chloride (14470-28-1) → C30H29N5O6 (1373391-49-1)

Guidance literature:

With pyridine;

DOI:10.1016/j.bmcl.2012.03.021

Reference yield:

C17H16IN5O5 (1019639-23-6) → C30H29N5O6 (1373391-49-1)

Guidance literature:

Multi-step reaction with 3 steps

1: ammonium bisulphate; 3-chloro-benzenecarboperoxoic acid / dichloromethane

2: ammonia / methanol

3: pyridine

With pyridine; ammonium bisulphate; ammonia; 3-chloro-benzenecarboperoxoic acid; In methanol; dichloromethane;

DOI:10.1016/j.bmcl.2012.03.021

Reference yield:

C10H12N2O4 (1019639-22-5) → C30H29N5O6 (1373391-49-1)

Guidance literature:

Multi-step reaction with 5 steps

1: benzyl triethylammonium azide; iodine; 4-methylmorpholine N-oxide / tetrahydrofuran

2: dmap / tetrahydrofuran; 1-methyl-pyrrolidin-2-one

3: ammonium bisulphate; 3-chloro-benzenecarboperoxoic acid / dichloromethane

4: ammonia / methanol

5: pyridine

With pyridine; dmap; ammonium bisulphate; benzyl triethylammonium azide; ammonia; iodine; 4-methylmorpholine N-oxide; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; methanol; dichloromethane;

DOI:10.1016/j.bmcl.2012.03.021

upstream raw materials:

C₁₀H₁₂N₂O₄

C₁₀H₁₂IN₅O₄

C₁₇H₁₆IN₅O₅

C₂₄H₂₀ClN₅O₇

Downstream raw materials:

C₃₄H₃₆N₆O₆

C₄₀H₄₇N₇O₈

C₃₄H₃₅N₅O₇

C₄₀H₄₆N₆O₉