π-tetramethylcyclobutadienedicarbonylcobalt-μ-phenyltelluride tungstenpentacarbonyl

Base Information

• Chemical Name: π-tetramethylcyclobutadienedicarbonylcobalt-μ-phenyltelluride tungstenpentacarbonyl
• CAS No.: 1131863-75-6
• Molecular Formula: C₂₁H₁₇CoO₇TeW
• Molecular Weight: 751.805
• Mol file: 1131863-75-6.mol

Synonyms:

Chemical Property of π-tetramethylcyclobutadienedicarbonylcobalt-μ-phenyltelluride tungstenpentacarbonyl

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of π-tetramethylcyclobutadienedicarbonylcobalt-μ-phenyltelluride tungstenpentacarbonyl

There total 1 articles about π-tetramethylcyclobutadienedicarbonylcobalt-μ-phenyltelluride tungstenpentacarbonyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 22.0%

tetrahydrofuran (109-99-9,24979-97-3,77392-70-2) + tungsten hexacarbonyl (14040-11-0) + dicarbonyliodo(tetramethylcyclobutadiene)cobalt(I) (12244-95-0) + diphenyl ditelluride (32294-60-3) → π-tetramethylcyclobutadienedicarbonylcobalt-μ-phenyltelluride tungstenpentacarbonyl (1131863-75-6)

Guidance literature:

With Na; In tetrahydrofuran; Irradiation (UV/VIS); (Ar); irradiation of THF soln. of tungsten compd. with UV for 40 min, treatment of sodium with tellurium compd. in THF, treatment of cobalt compd. with prepd. soln. of NaTePh, addn. of prepd. soln. of tungsten compd., stirring for 20 min; evapn., extn. (petroleum ether, diethyl ether of CH2Cl2), evapn., elem. anal.;

DOI:10.1007/s11172-007-0268-9

upstream raw materials:

tetrahydrofuran

tungsten hexacarbonyl

dicarbonyliodo(tetramethylcyclobutadiene)cobalt(I)

diphenyl ditelluride