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Technology Process of Tl(C6H3(CH(CH3)2)2N)2CN(CH(CH3)2)2

Tl(C6H3(CH(CH3)2)2N)2CN(CH(CH3)2)2

Base Information
  • Chemical Name:Tl(C6H3(CH(CH3)2)2N)2CN(CH(CH3)2)2
  • CAS No.:1036739-15-7
  • Molecular Formula:C31H48N3Tl
  • Molecular Weight:667.125
  • Hs Code.:
Tl(C<sub>6</sub>H<sub>3</sub>(CH(CH<sub>3</sub>)2)2N)2CN(CH(CH<sub>3</sub>)2)2

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Chemical Property of Tl(C6H3(CH(CH3)2)2N)2CN(CH(CH3)2)2
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Technology Process of Tl(C6H3(CH(CH3)2)2N)2CN(CH(CH3)2)2

There total 1 articles about Tl(C6H3(CH(CH3)2)2N)2CN(CH(CH3)2)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

thallium(I) bromide

thallium(I) bromide

[Li((2,6-diisopropylphenyl-N)2CNPr(i)2)]

[Li((2,6-diisopropylphenyl-N)2CNPr(i)2)]

Tl(C<sub>6</sub>H<sub>3</sub>(CH(CH<sub>3</sub>)2)2N)2CN(CH(CH<sub>3</sub>)2)2
1036739-15-7

Tl(C6H3(CH(CH3)2)2N)2CN(CH(CH3)2)2

Guidance literature:
In toluene; byproducts: LiBr; (under N2 or Ar, Schlenk); TlBr added to cooled ligand in toluene at -80°C, warmed to ambient temp. overnight with stirring; filtered, volatiles removed under reduced pressure, residue extd. with hexane, concd., slowly cooled to -30°C;
DOI:10.1039/b718799h
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