Technology Process of C17H17Cl2N7O4
There total 6 articles about C17H17Cl2N7O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1: dmap; N,N-dimethyl-ethanamine / acetonitrile / 1 h / 20 °C
2: tetraethylammonium chloride; N,N-dimethyl-aniline; trichlorophosphate / 100 °C
3: benzyltriethylammonium nitrite; acetyl chloride / dichloromethane / 1 h / 0 °C / Inert atmosphere; Cooling with ice
4: ammonia / ethanol / 72 h / 20 °C
5: hydrazine hydrate / 10 h / 20 °C
6: methanol / Reflux
With
dmap; benzyltriethylammonium nitrite; hydrazine hydrate; N,N-dimethyl-ethanamine; tetraethylammonium chloride; ammonia; N,N-dimethyl-aniline; acetyl chloride; trichlorophosphate;
In
methanol; ethanol; dichloromethane; acetonitrile;
DOI:10.1016/j.bmc.2012.11.021
- Guidance literature:
-
Multi-step reaction with 4 steps
1: benzyltriethylammonium nitrite; acetyl chloride / dichloromethane / 1 h / 0 °C / Inert atmosphere; Cooling with ice
2: ammonia / ethanol / 72 h / 20 °C
3: hydrazine hydrate / 10 h / 20 °C
4: methanol / Reflux
With
benzyltriethylammonium nitrite; hydrazine hydrate; ammonia; acetyl chloride;
In
methanol; ethanol; dichloromethane;
DOI:10.1016/j.bmc.2012.11.021