[Pd(NCC₆H₄C₆H₄O(CH₂)6OC₆H₃CHNC₆H₄OC₁₀H₂₁)(N,N-dipropyl-N'-benzoyl thiourea)]

Base Information

• Chemical Name: [Pd(NCC₆H₄C₆H₄O(CH₂)6OC₆H₃CHNC₆H₄OC₁₀H₂₁)(N,N-dipropyl-N'-benzoyl thiourea)]
• CAS No.: 1221071-56-2
• Molecular Formula: C₅₆H₆₈N₄O₄PdS
• Molecular Weight: 999.666
• Mol file: 1221071-56-2.mol

Synonyms:

Chemical Property of [Pd(NCC₆H₄C₆H₄O(CH₂)6OC₆H₃CHNC₆H₄OC₁₀H₂₁)(N,N-dipropyl-N'-benzoyl thiourea)]

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of [Pd(NCC₆H₄C₆H₄O(CH₂)6OC₆H₃CHNC₆H₄OC₁₀H₂₁)(N,N-dipropyl-N'-benzoyl thiourea)]

There total 1 articles about [Pd(NCC₆H₄C₆H₄O(CH₂)6OC₆H₃CHNC₆H₄OC₁₀H₂₁)(N,N-dipropyl-N'-benzoyl thiourea)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

N,N-di-n-propyl-N'-benzoyl thiourea sodium salt + [Pd(NCC6H4C6H4O(CH2)6OC6H3CHNC6H4OC10H21)(CH3COO)]2 (1221071-52-8) → [Pd(NCC6H4C6H4O(CH2)6OC6H3CHNC6H4OC10H21)(N,N-dipropyl-N'-benzoyl thiourea)] (1221071-56-2)

Guidance literature:

In dichloromethane; Na(C6H5CONSONPr2) salt added to soln. of binuclear complex of Pd in CH2Cl2; mixt. stirred at room temp. for 1 d and then solvent removed; residue purified on silica using CH2Cl2 as eluent; complex recrystd. from CH2Cl2/C2H5OH at -25°C; elem. anal.;

DOI:10.1016/j.ica.2009.11.028

upstream raw materials:

[Pd(NCC₆H₄C₆H₄O(CH₂)6OC₆H₃CHNC₆H₄OC₁₀H₂₁)(CH₃COO)]2