{Fe(CO)(⁽¹³⁾CO)(P(CH₃)3)2(NCCH₃)CH₃}⁽¹⁺⁾*B(C₆H₅)4^(1-)={Fe(CO)(⁽¹³⁾CO)(P(CH₃)3)2(NCCH₃)CH₃}B(C₆H₅)4

Base Information

• Chemical Name: {Fe(CO)(⁽¹³⁾CO)(P(CH₃)3)2(NCCH₃)CH₃}⁽¹⁺⁾*B(C₆H₅)4^(1-)={Fe(CO)(⁽¹³⁾CO)(P(CH₃)3)2(NCCH₃)CH₃}B(C₆H₅)4
• CAS No.: 141613-56-1
• Molecular Formula: C₁₁H₂₄FeNO₂P₂*C₂₄H₂₀B
• Molecular Weight: 640.334

Synonyms:

Chemical Property of {Fe(CO)(⁽¹³⁾CO)(P(CH₃)3)2(NCCH₃)CH₃}⁽¹⁺⁾*B(C₆H₅)4^(1-)={Fe(CO)(⁽¹³⁾CO)(P(CH₃)3)2(NCCH₃)CH₃}B(C₆H₅)4

Chemical Property:

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Safty Information:

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MSDS Files:

Useful:

Technology Process of {Fe(CO)(⁽¹³⁾CO)(P(CH₃)3)2(NCCH₃)CH₃}⁽¹⁺⁾*B(C₆H₅)4^(1-)={Fe(CO)(⁽¹³⁾CO)(P(CH₃)3)2(NCCH₃)CH₃}B(C₆H₅)4

There total 1 articles about {Fe(CO)(⁽¹³⁾CO)(P(CH₃)3)2(NCCH₃)CH₃}⁽¹⁺⁾*B(C₆H₅)4^(1-)={Fe(CO)(⁽¹³⁾CO)(P(CH₃)3)2(NCCH₃)CH₃}B(C₆H₅)4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

cis,trans-[dicarbonylbis(trimethylphosphine)(methyl)iodoiron(II)] (33542-07-3) + sodium tetraphenyl borate (143-66-8) → {Fe(CO)((13)CO)(P(CH3)3)2(NCCH3)CH3}(1+)*B(C6H5)4(1-)={Fe(CO)((13)CO)(P(CH3)3)2(NCCH3)CH3}B(C6H5)4 (141723-97-9) + {Fe(CO)((13)CO)(P(CH3)3)2(NCCH3)CH3}(1+)*B(C6H5)4(1-)={Fe(CO)((13)CO)(P(CH3)3)2(NCCH3)CH3}B(C6H5)4 (141613-56-1) + {Fe(CO)2(P(CH3)3)2(NCCH3)CH3}(1+)*B(C6H5)4(1-)={Fe(CO)2(P(CH3)3)2(NCCH3)CH3}B(C6H5)4 (89616-73-9)

Guidance literature:

With acetonitrile; In hexane; (Fe(CO)2(PMe3)2MeI) was reacted in n-hexane at 30 °C with (13)CO for 6h; no labeling of the acetyl substituent was observed by IR; decarbonylation of the acetyl in n-hexane at 30 °C for 2h gave a mixture of neutral labeled Fe-complexes;; the obtained mixture was dissolved in methanol containing NaBPh4, to the stirred soln. CH3CN was added, after few minutes a white solid pptd., filtered, washed with CH3OH and dried (about 40 % yield); product mixture obtained; (31)P-NMR;;

Reference yield:

{Fe(CO)((13)CO)(P(CH3)3)2(NCCH3)CH3}(1+)*B(C6H5)4(1-)={Fe(CO)((13)CO)(P(CH3)3)2(NCCH3)CH3}B(C6H5)4 (141613-56-1) → {Fe(CO)((13)CO)(P(CH3)3)2(NCCH3)CH3}(1+)*B(C6H5)4(1-)={Fe(CO)((13)CO)(P(CH3)3)2(NCCH3)CH3}B(C6H5)4 (141723-97-9)

Guidance literature:

In acetonitrile; isotopomerization in CH3CN;; IR;;

upstream raw materials:

cis,trans-[dicarbonylbis(trimethylphosphine)(methyl)iodoiron(II)]

sodium tetraphenyl borate

Downstream raw materials:

{Fe(CO)(⁽¹³⁾CO)(P(CH₃)3)2(NCCH₃)CH₃}⁽¹⁺⁾*B(C₆H₅)4^(1-)={Fe(CO)(⁽¹³⁾CO)(P(CH₃)3)2(NCCH₃)CH₃}B(C₆H₅)4

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