(1,2-bis(diphenylphosphino)ethane)Pt(n-C₃F₇)OTf

Base Information

Chemical Name:(1,2-bis(diphenylphosphino)ethane)Pt(n-C₃F₇)OTf
CAS No.:364376-68-1
Molecular Formula:C₃₀H₂₄F₁₀O₃P₂PtS
Molecular Weight:911.596
Hs Code.:

(1,2-bis(diphenylphosphino)ethane)Pt(n-C<sub>3</sub>F<sub>7</sub>)OTf

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Chemical Property of (1,2-bis(diphenylphosphino)ethane)Pt(n-C₃F₇)OTf

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Technology Process of (1,2-bis(diphenylphosphino)ethane)Pt(n-C₃F₇)OTf

There total 2 articles about (1,2-bis(diphenylphosphino)ethane)Pt(n-C₃F₇)OTf which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 364376-67-0
(1,2-bis(diphenylphosphino)ethane)Pt(n-C₃F₇)(CH₃)

: 1493-13-6
trifluorormethanesulfonic acid

: 364376-68-1
(1,2-bis(diphenylphosphino)ethane)Pt(n-C₃F₇)OTf

Guidance literature:: In dichloromethane; under N2 atm. CF3SO3H was added to soln.(DPPE)Pt(n-C3F7)(CH3) in CH2Cl2 and stirred for 16 h; soln. was concd. in vacuo, residue was dissolved in CH2Cl2, filtered through Celite, toluene was added, CH2Cl2 was removed in vacuo, ppt. was washed with toluene; elem. anal.;
DOI:10.1021/om010424h

Reference yield:

: 1663-45-2
1,2-bis-(diphenylphosphino)ethane

: 364376-68-1
(1,2-bis(diphenylphosphino)ethane)Pt(n-C₃F₇)OTf

Guidance literature:: Multi-step reaction with 2 steps

1: toluene

2: dichloromethane

In dichloromethane; toluene;
DOI:10.1021/om010424h

Reference yield: 97.0%

: 364376-68-1
(1,2-bis(diphenylphosphino)ethane)Pt(n-C₃F₇)OTf

: 7681-82-5,24359-64-6,41927-88-2,115813-40-6
sodium iodide

: 364376-71-6
(1,2-bis(diphenylphosphino)ethane)Pt(n-C₃F₇)I

Guidance literature:: In dichloromethane; water; under N2 atm. to soln. (DPPE)Pt(n-C3F7)OTf in moist CH2Cl2 was added aq.soln. NaI and stirred for 16 h; org. layer was separated, dried over MgSO4 and filtered through Celite, solvent was removed in vacuo, residue was washed with EtOH and hexane; elem. anal.;
DOI:10.1021/om010424h