[Fe(C₅H₅)(C₅H₃C₄H₂N₂(NHC₆H₄NO₂))PdCl(P(C₆H₅)3)]

Base Information

• Chemical Name: [Fe(C₅H₅)(C₅H₃C₄H₂N₂(NHC₆H₄NO₂))PdCl(P(C₆H₅)3)]
• CAS No.: 1350659-36-7
• Molecular Formula: C₃₈H₃₀ClFeN₄O₂PPd
• Molecular Weight: 803.376
• Mol file: 1350659-36-7.mol

Synonyms:

Chemical Property of [Fe(C₅H₅)(C₅H₃C₄H₂N₂(NHC₆H₄NO₂))PdCl(P(C₆H₅)3)]

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of [Fe(C₅H₅)(C₅H₃C₄H₂N₂(NHC₆H₄NO₂))PdCl(P(C₆H₅)3)]

There total 1 articles about [Fe(C₅H₅)(C₅H₃C₄H₂N₂(NHC₆H₄NO₂))PdCl(P(C₆H₅)3)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

[PdCl[(η5-C5H5)Fe(η5-C5H3)-N2C4H2Cl]PPh3] (1252932-00-5) + 4-nitro-aniline (100-01-6,104810-17-5) → [Fe(C5H5)(C5H3C4H2N2(NHC6H4NO2))PdCl(P(C6H5)3)] (1350659-36-7)

Guidance literature:

In 1,4-dioxane; Schlenk technique, under N2: react. of Pd complex (0.5 mmol) and NH2C6H4NO2 (0.75 mmol) at 110°C for 24 h; organic layer sepd., aq. layer extracted with CH2Cl2, combined organic layer washed with H2O, dried with MgSO4, filtered, solvent evapd., chromd. (silica gel);

DOI:10.1002/ejic.201100617

upstream raw materials:

[PdCl[(η5-C5H5)Fe(η5-C5H3)-N2C4H2Cl]PPh3]

4-nitro-aniline