{(C₅H₅)Mo(SCHC((C₆H₅))S)}2

Base Information

Chemical Name:{(C₅H₅)Mo(SCHC((C₆H₅))S)}2
CAS No.:72186-27-7
Molecular Formula:C₂₆H₂₂Mo₂S₄
Molecular Weight:654.605
Hs Code.:

{(C<sub>5</sub>H<sub>5</sub>)Mo(SCHC((C<sub>6</sub>H<sub>5</sub>))S)}2

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of {(C₅H₅)Mo(SCHC((C₆H₅))S)}2

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Technology Process of {(C₅H₅)Mo(SCHC((C₆H₅))S)}2

There total 1 articles about {(C₅H₅)Mo(SCHC((C₆H₅))S)}2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 75675-64-8
{CpMo(μ-S)(μ-SH)}2

: 536-74-3
phenylacetylene

: 72186-27-7
{(C₅H₅)Mo(SCHC((C₆H₅))S)}2

: CpMo(O)(μ-S)2Mo(SCHC(Ph)S)Cp

Guidance literature:: With air; In dichloromethane; phenylacetylene syringed into soln. of {CpMo(μ-S)(μ-SH)}2 in CH2Cl2; soln. 24 h stirred under air at ambient temp. (color change to dark green); solvent removed; product mixt. chromd. on alumina with hexane/CH2Cl2 giving yellow fraction contg. bis(phenylacetylene) adduct and green-blue fraction with desired anti-CpMoO(μ-S)2Mo(SCHC(Ph)S)Cp; solvent removed; powder recrystd. from Et2O; elem. anal.;

Reference yield:

: 72186-27-7
{(C₅H₅)Mo(SCHC((C₆H₅))S)}2

: CpMo(O)(μ-S)2Mo(SCHC(Ph)S)Cp

Guidance literature:: With trifluoroacetic acid; air; In dichloromethane; trifluoroacetic acid syringed into soln. of {CpMo(SCHC(Ph)S)}2; soln. stirred under air (7 d, ambient temp.);; solvent removed; chromy. of product mixt. on alumina with hexane/CH2Cl2 giving yellow-green fraction contg. anti-isomer (spect. anal.) and light violet fraction contg. syn-isomer (recrystd. from Et2O/CH2Cl2, elem. anal.);