1,2,7,8-Re₂Cl₄(PMe₂Ph)4

Base Information

Chemical Name:1,2,7,8-Re₂Cl₄(PMe₂Ph)4
CAS No.:85993-34-6
Molecular Formula:C₃₂H₄₄Cl₄P₄Re₂
Molecular Weight:1066.82
Hs Code.:

1,2,7,8-Re<sub>2</sub>Cl<sub>4</sub>(PMe<sub>2</sub>Ph)4

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Chemical Property of 1,2,7,8-Re₂Cl₄(PMe₂Ph)4

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Technology Process of 1,2,7,8-Re₂Cl₄(PMe₂Ph)4

There total 4 articles about 1,2,7,8-Re₂Cl₄(PMe₂Ph)4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: Re₂(OOCCH₃)Cl₄(P(C₆H₅)3)2

: 672-66-2
Dimethyl(phenyl)phosphine

: 85993-34-6,204336-50-5,67554-13-6
1,2,7,8-Re₂Cl₄(PMe₂Ph)4

Guidance literature:: In dichloromethane; CH2Cl2 soln. of Re-complex was treated with ligand, stirred for 8 h at room temp. under N2; solvent was removed under reduced pressure, washed with pentane, extd. with benzene;
DOI:10.1039/b005975g

Reference yield: 78.0%

: 1,2,7-Re₂Cl₅(PMe₂Ph)3

: 672-66-2
Dimethyl(phenyl)phosphine

: 85993-34-6,204336-50-5,67554-13-6
1,2,7,8-Re₂Cl₄(PMe₂Ph)4

Guidance literature:: With Cp₂Co; In dichloromethane; byproducts: [Cp2Co]Cl; inert atmosphere; stirring Re-complex with slight excess Cp2Co at room temp. for 1 h, addn. of phosphine, stirring for 1 h; vol. reduction, C6H6 addn., filtration off of Cp2CoCl, solvent removal (reduced pressure);