Technology Process of C21H27BO12
There total 5 articles about C21H27BO12 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: boron trifluoride diethyl etherate / dichloromethane / 18 h / 0 - 20 °C / Inert atmosphere
2: potassium acetate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,4-dioxane / 18 °C / Inert atmosphere; Reflux
3: diethyl ether / 18 h
4: hydrogenchloride / diethyl ether / 2 h
With
hydrogenchloride; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; boron trifluoride diethyl etherate; potassium acetate;
In
1,4-dioxane; diethyl ether; dichloromethane;
DOI:10.1039/c3cc38824g
- Guidance literature:
-
With
hydrogenchloride;
In
diethyl ether;
for 2h;
DOI:10.1039/c3cc38824g
- Guidance literature:
-
Multi-step reaction with 3 steps
1: potassium acetate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,4-dioxane / 18 °C / Inert atmosphere; Reflux
2: diethyl ether / 18 h
3: hydrogenchloride / diethyl ether / 2 h
With
hydrogenchloride; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate;
In
1,4-dioxane; diethyl ether;
DOI:10.1039/c3cc38824g