2,4-bis(dec-9-enyloxy)-1-iodobenzene

Base Information

Chemical Name:2,4-bis(dec-9-enyloxy)-1-iodobenzene
CAS No.:1172640-30-0
Molecular Formula:C₂₆H₄₁IO₂
Molecular Weight:512.515
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,4-bis(dec-9-enyloxy)-1-iodobenzene

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Technology Process of 2,4-bis(dec-9-enyloxy)-1-iodobenzene

There total 1 articles about 2,4-bis(dec-9-enyloxy)-1-iodobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 22.0%

: 13019-22-2
9-Decen-1-ol

: 41046-68-8
4-iodobenzene-1,3-diol

: 1172640-30-0
2,4-bis(dec-9-enyloxy)-1-iodobenzene

Guidance literature:: 9-Decen-1-ol; 4-iodobenzene-1,3-diol; With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 20 ℃; for 18h; Inert atmosphere;

With sodium hydroxide; water; In tetrahydrofuran; for 0.5h;
DOI:10.1002/ejoc.200801261

Reference yield:

: 1172640-30-0
2,4-bis(dec-9-enyloxy)-1-iodobenzene

: 1172640-33-3
2,4-bis(dec-9-enyloxy)phenylboronic acid

Guidance literature:: 2,4-bis(dec-9-enyloxy)-1-iodobenzene; With n-butyllithium; In tetrahydrofuran; Petroleum ether; at -78 ℃; for 1h; Inert atmosphere;

With Trimethyl borate; In tetrahydrofuran; Petroleum ether; at -78 - 20 ℃; for 2h; Inert atmosphere;

With water; In tetrahydrofuran; Petroleum ether; at 20 ℃;
DOI:10.1002/ejoc.200801261