C₁₄H₁₇BrO₂Zn

Base Information

Chemical Name:C₁₄H₁₇BrO₂Zn
CAS No.:1447729-04-5
Molecular Formula:C₁₄H₁₇BrO₂Zn
Molecular Weight:362.582
Hs Code.:

C<sub>14</sub>H<sub>17</sub>BrO<sub>2</sub>Zn

Synonyms:

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Chemical Property of C₁₄H₁₇BrO₂Zn

Chemical Property:

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Technology Process of C₁₄H₁₇BrO₂Zn

There total 6 articles about C₁₄H₁₇BrO₂Zn which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1447728-78-0
C₁₄H₁₇BrO₂

: 7699-45-8
zinc dibromide

: 1447729-04-5
C₁₄H₁₇BrO₂Zn

Guidance literature:: With naphthalene; trimethylsilyl bromide; lithium; In tetrahydrofuran; at 20 ℃; for 19h; Reagent/catalyst; Inert atmosphere; Sonication;
DOI:10.1016/j.tetlet.2013.05.114

Reference yield:

: 1447728-67-7
C₁₃H₁₈Se

: 1447729-04-5
C₁₄H₁₇BrO₂Zn

Guidance literature:: Multi-step reaction with 4 steps

1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 1 h / -78 °C / Inert atmosphere

2: sodium benzoate / toluene / 1 h / 100 °C / Inert atmosphere

3: Phenylselenyl bromide / dichloromethane / 5 h / -45 - 0 °C / Inert atmosphere

4: lithium; naphthalene; trimethylsilyl bromide / tetrahydrofuran / 19 h / 20 °C / Inert atmosphere; Sonication

With sodium benzoate; naphthalene; trimethylsilyl bromide; Phenylselenyl bromide; lithium; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane; toluene;
DOI:10.1016/j.tetlet.2013.05.114

Reference yield:

: 766-00-7
2-cyclopentyl-ethanol

: 1447729-04-5
C₁₄H₁₇BrO₂Zn

Guidance literature:: Multi-step reaction with 6 steps

1: triethylamine / tetrahydrofuran / 1 h / 0 - 20 °C / Inert atmosphere

2: sodium tetrahydroborate / methanol / 3 h / Inert atmosphere

3: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 1 h / -78 °C / Inert atmosphere

4: sodium benzoate / toluene / 1 h / 100 °C / Inert atmosphere

5: Phenylselenyl bromide / dichloromethane / 5 h / -45 - 0 °C / Inert atmosphere

6: lithium; naphthalene; trimethylsilyl bromide / tetrahydrofuran / 19 h / 20 °C / Inert atmosphere; Sonication

With sodium benzoate; sodium tetrahydroborate; naphthalene; trimethylsilyl bromide; Phenylselenyl bromide; lithium; triethylamine; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; methanol; dichloromethane; toluene;
DOI:10.1016/j.tetlet.2013.05.114