C₂₆H₃₅GaGe

Base Information

• Chemical Name: C₂₆H₃₅GaGe
• CAS No.: 1613379-01-3
• Molecular Formula: C₂₆H₃₅GaGe
• Molecular Weight: 489.877
• Mol file: 1613379-01-3.mol

Synonyms:

Chemical Property of C₂₆H₃₅GaGe

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₆H₃₅GaGe

There total 2 articles about C₂₆H₃₅GaGe which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

di(tert-butyl)gallium hydride (378795-11-0) + (H5C6)2Ge(C≡C-CMe)2 (1613378-90-7) → C26H35GaGe (1613379-01-3)

Guidance literature:

In toluene; at 0 - 20 ℃; for 3h; Inert atmosphere;

DOI:10.1002/ejic.201402132

Reference yield:

dichlorodiphenylgermane (1613-66-7) → C26H35GaGe (1613379-01-3)

Guidance literature:

Multi-step reaction with 2 steps

1: diethyl ether; tetrahydrofuran / 2 h / 0 °C / Reflux; Inert atmosphere

2: toluene / 3 h / 0 - 20 °C / Inert atmosphere

In tetrahydrofuran; diethyl ether; toluene;

DOI:10.1002/ejic.201402132

upstream raw materials:

dichlorodiphenylgermane

di(tert-butyl)gallium hydride

(H₅C₆)₂Ge(C≡C-CMe)₂