Technology Process of C31H48N6O2
There total 6 articles about C31H48N6O2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
chlorotriisopropylsilane; water; trifluoroacetic acid;
In
dichloromethane;
at 20 ℃;
for 2h;
DOI:10.1021/jm901052r
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: triethylamine / water; 1,4-dioxane / 18 h / 20 °C / pH 8
2.1: lithium hydroxide; water / 1,4-dioxane / 18 h / 100 °C
3.1: fluoro-N,N,N',N'-tetramethylformamidinium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 °C
3.2: 168 h / 20 °C
4.1: trifluoroacetic acid; chlorotriisopropylsilane / dichloromethane; water / 2 h / 20 °C
With
chlorotriisopropylsilane; water; triethylamine; N-ethyl-N,N-diisopropylamine; fluoro-N,N,N',N'-tetramethylformamidinium hexafluorophosphate; trifluoroacetic acid; lithium hydroxide;
In
1,4-dioxane; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2012.09.048
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: lithium hydroxide; water / 1,4-dioxane / 18 h / 100 °C
2.1: fluoro-N,N,N',N'-tetramethylformamidinium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 °C
2.2: 168 h / 20 °C
3.1: trifluoroacetic acid; chlorotriisopropylsilane / dichloromethane; water / 2 h / 20 °C
With
chlorotriisopropylsilane; water; N-ethyl-N,N-diisopropylamine; fluoro-N,N,N',N'-tetramethylformamidinium hexafluorophosphate; trifluoroacetic acid; lithium hydroxide;
In
1,4-dioxane; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2012.09.048