cyclopenta-2,4-dien-1-yl-dimethyl(phenylethynyl)silane

Base Information

Chemical Name:cyclopenta-2,4-dien-1-yl-dimethyl(phenylethynyl)silane
CAS No.:1234615-03-2
Molecular Formula:C₁₅H₁₆Si
Molecular Weight:224.378
Hs Code.:

Synonyms:

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Chemical Property of cyclopenta-2,4-dien-1-yl-dimethyl(phenylethynyl)silane

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Technology Process of cyclopenta-2,4-dien-1-yl-dimethyl(phenylethynyl)silane

There total 2 articles about cyclopenta-2,4-dien-1-yl-dimethyl(phenylethynyl)silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6738-06-3
phenylethynylmagnesium bromide

: sodium cyclopentadienide

: 75-78-5,30107-43-8
dimethylsilicon dichloride

: 1234615-03-2
cyclopenta-2,4-dien-1-yl-dimethyl(phenylethynyl)silane

: 1234615-13-4
cyclopenta-2,4-dien-2-yl-dimethyl(phenylethynyl)silane

Guidance literature:: sodium cyclopentadienide; dimethylsilicon dichloride;

phenylethynylmagnesium bromide; In diethyl ether; at 20 ℃; Inert atmosphere; Reflux;
DOI:10.1002/ejic.200900769

Reference yield:

: lithium cyclopentadienide

: 75-78-5,30107-43-8
dimethylsilicon dichloride

: 4440-01-1
lithium phenylacetylide

: 1234615-03-2
cyclopenta-2,4-dien-1-yl-dimethyl(phenylethynyl)silane

: 1234615-13-4
cyclopenta-2,4-dien-2-yl-dimethyl(phenylethynyl)silane

: 1234615-14-5
C₁₅H₁₆Si

Guidance literature:: lithium cyclopentadienide; dimethylsilicon dichloride; In tetrahydrofuran; at -40 - 20 ℃;

lithium phenylacetylide; In tetrahydrofuran; at -40 ℃; for 15h;
DOI:10.1139/V10-129

Reference yield: 39.0%

: 15226-74-1,61091-28-9,61117-58-6
dicobalt octacarbonyl

: 1234615-03-2
cyclopenta-2,4-dien-1-yl-dimethyl(phenylethynyl)silane

: 1234615-07-6
[μ-(cyclopenta-2,4-dien-1-yl)[(1,2-η:1,2-η)-phenylethynyl]silane]bis[tricarbonylcobalt(0)]

Guidance literature:: In hexane; byproducts: CO; (Ar), Co complex dissolved in hexane added under stirring at room temp. to soln. of ligand (1:1) in hexane, reacted for 1 d; concd.(vac.), cooled to -78°C, warmed to -20°C, pptd., washed (hexane), dried (vac.), elem. anal.;
DOI:10.1002/ejic.200900769