(E)-ethyl propylidene phenylacetic carboxylate

Base Information

Chemical Name:(E)-ethyl propylidene phenylacetic carboxylate
CAS No.:82234-61-5
Molecular Formula:C₁₃H₁₆O₂
Molecular Weight:204.269
Hs Code.:

Synonyms:

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Chemical Property of (E)-ethyl propylidene phenylacetic carboxylate

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Technology Process of (E)-ethyl propylidene phenylacetic carboxylate

There total 3 articles about (E)-ethyl propylidene phenylacetic carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 65946-52-3
1-Ethoxy-1-trimethylsilyloxy-1-buten

: 82234-61-5
(E)-ethyl propylidene phenylacetic carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) methyllithium / diethyl ether / 1.) 0 deg C, 1 h, 2.) room temperature, 1 h

2: phenothiazine / toluene / 14 h / Heating

With 10H-phenothiazine; methyllithium; In diethyl ether; toluene;

Reference yield:

: 105-54-4
butanoic acid ethyl ester

: 82234-61-5
(E)-ethyl propylidene phenylacetic carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) LDA / tetrahydrofuran / 1.) -78 deg C, 40 min, 2.) -78 deg C, 25 min, 3.) room temperature, 1 h

2: 1.) methyllithium / diethyl ether / 1.) 0 deg C, 1 h, 2.) room temperature, 1 h

3: phenothiazine / toluene / 14 h / Heating

With 10H-phenothiazine; methyllithium; lithium diisopropyl amide; In tetrahydrofuran; diethyl ether; toluene;