(S)-2-((S)-2-Amino-3-benzyloxycarbonyl-propionylamino)-6-benzyloxycarbonylamino-hexanoic acid benzyl ester; compound with trifluoro-acetic acid

Base Information

• Chemical Name: (S)-2-((S)-2-Amino-3-benzyloxycarbonyl-propionylamino)-6-benzyloxycarbonylamino-hexanoic acid benzyl ester; compound with trifluoro-acetic acid
• CAS No.: 65001-84-5
• Molecular Formula: C₂HF₃O₂*C₃₂H₃₇N₃O₇
• Molecular Weight: 689.686

Synonyms:

Chemical Property of (S)-2-((S)-2-Amino-3-benzyloxycarbonyl-propionylamino)-6-benzyloxycarbonylamino-hexanoic acid benzyl ester; compound with trifluoro-acetic acid

Chemical Property:

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Technology Process of (S)-2-((S)-2-Amino-3-benzyloxycarbonyl-propionylamino)-6-benzyloxycarbonylamino-hexanoic acid benzyl ester; compound with trifluoro-acetic acid

There total 2 articles about (S)-2-((S)-2-Amino-3-benzyloxycarbonyl-propionylamino)-6-benzyloxycarbonylamino-hexanoic acid benzyl ester; compound with trifluoro-acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

BocD(OBzl)K(Z)OBzl (33838-60-7) + trifluoroacetic acid (76-05-1) → (S)-2-((S)-2-Amino-3-benzyloxycarbonyl-propionylamino)-6-benzyloxycarbonylamino-hexanoic acid benzyl ester; compound with trifluoro-acetic acid (65001-84-5)

Guidance literature:

In dichloromethane; Ambient temperature;

DOI:10.1021/jm00170a012

Reference yield:

→ 4-Benzyl-Asp-N6-Z-Lys-O-CH2Ph-trifluoressigsaeure (65001-84-5)

Guidance literature:

N-BOC-Derivat IV, Trifluoressigsaeure, Zwischenprodukt;

Reference yield:

(S)-2-((S)-2-Amino-3-benzyloxycarbonyl-propionylamino)-6-benzyloxycarbonylamino-hexanoic acid benzyl ester; compound with trifluoro-acetic acid (65001-84-5) → Cyclo (L-lys(Z)-L-Asp(OBzl)) (104371-57-5)

Guidance literature:

With 4-methyl-morpholine; acetic acid; In iso-butanol; Heating;

DOI:10.1016/S0040-4020(02)01021-9

upstream raw materials:

BocD(OBzl)K(Z)OBzl

trifluoroacetic acid

Downstream raw materials:

Cyclo (L-lys(Z)-L-Asp(OBzl))

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