Technology Process of C15H19F3O6S
There total 1 articles about C15H19F3O6S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
2,6-dimethylpyridine;
In
dichloromethane;
at -40 ℃;
for 0.5h;
DOI:10.1021/jo4025545
- Guidance literature:
-
C15H19F3O6S;
With
copper(l) iodide;
In
diethyl ether;
at -50 ℃;
for 0.166667h;
allylmagnesium bromide;
In
diethyl ether;
at -50 ℃;
for 1h;
DOI:10.1021/jo4025545
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: copper(l) iodide / diethyl ether / 0.17 h / -50 °C
1.2: 1 h / -50 °C
2.1: Hoveyda-Grubbs catalyst second generation / dichloromethane / 20 °C
3.1: diisobutylaluminium hydride / dichloromethane; hexane / 1 h / -78 °C
4.1: titanium(IV) isopropylate; diethyl (2S,3S)-tartrate / dichloromethane / 0.5 h / -20 °C / Molecular sieve
4.2: 8 h / -20 °C / Molecular sieve
5.1: 1H-imidazole; triphenylphosphine; iodine / tetrahydrofuran / 0.25 h / 20 °C
6.1: zinc; acetic acid / ethanol / 0.33 h / 20 °C
With
1H-imidazole; titanium(IV) isopropylate; copper(l) iodide; Hoveyda-Grubbs catalyst second generation; diethyl (2S,3S)-tartrate; iodine; diisobutylaluminium hydride; acetic acid; triphenylphosphine; zinc;
In
tetrahydrofuran; diethyl ether; ethanol; hexane; dichloromethane;
DOI:10.1021/jo4025545