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C15H19F3O6S

Base Information
  • Chemical Name:C15H19F3O6S
  • CAS No.:299402-17-8
  • Molecular Formula:C15H19F3O6S
  • Molecular Weight:384.373
  • Hs Code.:
C<sub>15</sub>H<sub>19</sub>F<sub>3</sub>O<sub>6</sub>S

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Chemical Property of C15H19F3O6S
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Technology Process of C15H19F3O6S

There total 1 articles about C15H19F3O6S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With 2,6-dimethylpyridine; In dichloromethane; at -40 ℃; for 0.5h;
DOI:10.1021/jo4025545
Guidance literature:
C15H19F3O6S; With copper(l) iodide; In diethyl ether; at -50 ℃; for 0.166667h;
allylmagnesium bromide; In diethyl ether; at -50 ℃; for 1h;
DOI:10.1021/jo4025545
Guidance literature:
Multi-step reaction with 6 steps
1.1: copper(l) iodide / diethyl ether / 0.17 h / -50 °C
1.2: 1 h / -50 °C
2.1: Hoveyda-Grubbs catalyst second generation / dichloromethane / 20 °C
3.1: diisobutylaluminium hydride / dichloromethane; hexane / 1 h / -78 °C
4.1: titanium(IV) isopropylate; diethyl (2S,3S)-tartrate / dichloromethane / 0.5 h / -20 °C / Molecular sieve
4.2: 8 h / -20 °C / Molecular sieve
5.1: 1H-imidazole; triphenylphosphine; iodine / tetrahydrofuran / 0.25 h / 20 °C
6.1: zinc; acetic acid / ethanol / 0.33 h / 20 °C
With 1H-imidazole; titanium(IV) isopropylate; copper(l) iodide; Hoveyda-Grubbs catalyst second generation; diethyl (2S,3S)-tartrate; iodine; diisobutylaluminium hydride; acetic acid; triphenylphosphine; zinc; In tetrahydrofuran; diethyl ether; ethanol; hexane; dichloromethane;
DOI:10.1021/jo4025545
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