1-DEOXY-D-RIBULOSE

Base Information

• Chemical Name: 1-DEOXY-D-RIBULOSE
• CAS No.: 148979-72-0
• Molecular Formula: C₆H₁₂O₄
• Molecular Weight: 148.159

Synonyms:

Chemical Property of 1-DEOXY-D-RIBULOSE

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

1-Deoxy-D-ribulose ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Uses: 1-Deoxy-D-ribulose (cas# 148979-72-0) is a compound useful in organic synthesis.

Technology Process of 1-DEOXY-D-RIBULOSE

There total 14 articles about 1-DEOXY-D-RIBULOSE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

(Z)-(4R,5R)-1-n-butylamino-5-hydroxy-4,6-O-dibenzyl-hex-1-en-3-one (1187452-05-6) → 1,2-dideoxy-D-threohex-3-ulose (1187452-09-0,148979-72-0)

Guidance literature:

With 5%-palladium/activated carbon; hydrogen; In methanol; at 20 ℃; for 4h;

DOI:10.1016/j.tetlet.2009.06.112

Reference yield: 93.0%

(Z)-(4S,5R)-1-n-butylamino-5-hydroxy-4,6-O-dibenzyl-hex-1-en-3-one (1187452-03-4) → 1,2-dideoxy-D-erythro-3-hexulose (148979-72-0)

Guidance literature:

With 5%-palladium/activated carbon; hydrogen; In methanol; at 20 ℃; for 4h;

DOI:10.1016/j.tetlet.2009.06.112

Reference yield: 90.0%

1-ethyl-(3,4-O-isopropylidene)-L-threose → 1-ethyl-L-threose (148979-72-0)

Guidance literature:

With acetic acid; In water; at 20 ℃;

DOI:10.1016/j.tetasy.2016.11.008

upstream raw materials:

3,4:5,6-di-O-isopropylidene-D-glucose diethyl dithioacetal

1-deoxy-3,4:5,6-di-O-isopropylidene-D-arabino-hex-2-ulose

(S)-1-[(4R,4'R,5'R)-2,2,2'-tetramethyl-4,4'-bi(1,3-dioxolan)-5-yl]ethanol

(Z)-(4S,5R)-1-benzylamino-5-hydroxy-4,6-O-dibenzyl-hex-1-en-3-one

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