C₃₉H₅₆INO₄Si

Base Information

Chemical Name:C₃₉H₅₆INO₄Si
CAS No.:1404379-98-1
Molecular Formula:C₃₉H₅₆INO₄Si
Molecular Weight:757.868
Hs Code.:

C<sub>39</sub>H<sub>56</sub>INO<sub>4</sub>Si

Synonyms:

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Chemical Property of C₃₉H₅₆INO₄Si

Chemical Property:

Purity/Quality:

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Technology Process of C₃₉H₅₆INO₄Si

There total 23 articles about C₃₉H₅₆INO₄Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 646-07-1
4-Methylpentanoic acid

: 1404379-98-1
C₃₉H₅₆INO₄Si

Guidance literature:: Multi-step reaction with 12 steps

1.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 20 °C

2.1: 1,1,3,3-Tetramethyldisiloxane / (Ph₃P)2IrCl(CO) / toluene / 2 h / 20 °C

3.1: hydroquinone / acetonitrile / 95 °C

4.1: methyl p-toluene sulfonate / water / 2 h / 110 °C

4.2: 4 h / 95 °C

5.1: hydrogen / rhodium contaminated with carbon / tetrahydrofuran / 7 h / 20 °C / 760.05 Torr

6.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 20 °C

7.1: diisobutylaluminium hydride / dichloromethane / 2 h / -78 °C

7.2: Cooling with ice

8.1: triphenylphosphine / dichloromethane / 0.33 h / Cooling with ice

8.2: 0.33 h / Cooling with ice

9.1: n-butyllithium / tetrahydrofuran

10.1: 1H-imidazole / N,N-dimethyl-formamide

11.1: pyridine / methanol

12.1: Iodine monochloride / dichloromethane

With pyridine; 1H-imidazole; n-butyllithium; 1,1,3,3-Tetramethyldisiloxane; hydrogen; Iodine monochloride; diisobutylaluminium hydride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; hydroquinone; methyl p-toluene sulfonate; triphenylphosphine; rhodium contaminated with carbon; (Ph₃P)2IrCl(CO); In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; toluene; acetonitrile;

Reference yield:

: 96556-40-0
methyl-3-(benzyloxy)-2.2-dimethylpropionate

: 1404379-98-1
C₃₉H₅₆INO₄Si

Guidance literature:: Multi-step reaction with 13 steps

1: lithium borohydride / tetrahydrofuran

2: triethylamine; pyridine-SO₃ complex / dichloromethane; dimethyl sulfoxide

3: toluene

4: sodium tetrahydroborate; methanol / cobalt(II) chloride hexahydrate / N,N-dimethyl-formamide

5: sodium hydroxide / ethanol

6: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / chloroform

7: tetrahydrofuran

8: palladium on activated charcoal / tetrahydrofuran

9: potassium tert-butylate / toluene

10: n-butyllithium / tetrahydrofuran

11: 1H-imidazole / N,N-dimethyl-formamide

12: pyridine / methanol

13: Iodine monochloride / dichloromethane

With pyridine; 1H-imidazole; methanol; dmap; sodium tetrahydroborate; lithium borohydride; n-butyllithium; pyridine-SO₃ complex; Iodine monochloride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; sodium hydroxide; cobalt(II) chloride hexahydrate; palladium on activated charcoal; potassium tert-butylate; In tetrahydrofuran; methanol; ethanol; dichloromethane; chloroform; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene;

Reference yield:

: 14002-80-3
Methyl 2,2-dimethyl-3-hydroxypropionate

: 1404379-98-1
C₃₉H₅₆INO₄Si

Guidance literature:: Multi-step reaction with 14 steps

1: diethyl ether

2: lithium borohydride / tetrahydrofuran

3: triethylamine; pyridine-SO₃ complex / dichloromethane; dimethyl sulfoxide

4: toluene

5: sodium tetrahydroborate; methanol / cobalt(II) chloride hexahydrate / N,N-dimethyl-formamide

6: sodium hydroxide / ethanol

7: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / chloroform

8: tetrahydrofuran

9: palladium on activated charcoal / tetrahydrofuran

10: potassium tert-butylate / toluene

11: n-butyllithium / tetrahydrofuran

12: 1H-imidazole / N,N-dimethyl-formamide

13: pyridine / methanol

14: Iodine monochloride / dichloromethane

With pyridine; 1H-imidazole; methanol; dmap; sodium tetrahydroborate; lithium borohydride; n-butyllithium; pyridine-SO₃ complex; Iodine monochloride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; sodium hydroxide; cobalt(II) chloride hexahydrate; palladium on activated charcoal; potassium tert-butylate; In tetrahydrofuran; methanol; diethyl ether; ethanol; dichloromethane; chloroform; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene;