C₃₆H₃₂N₄O₇S

Base Information

Chemical Name:C₃₆H₃₂N₄O₇S
CAS No.:745020-01-3
Molecular Formula:C₃₆H₃₂N₄O₇S
Molecular Weight:664.739
Hs Code.:

C<sub>36</sub>H<sub>32</sub>N<sub>4</sub>O<sub>7</sub>S

Synonyms:

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Chemical Property of C₃₆H₃₂N₄O₇S

Chemical Property:

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Technology Process of C₃₆H₃₂N₄O₇S

There total 8 articles about C₃₆H₃₂N₄O₇S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1448959-28-1
C₁₃H₁₇NO₃

: 745020-01-3
C₃₆H₃₂N₄O₇S

Guidance literature:: Multi-step reaction with 8 steps

1.1: hydrogenchloride / 48 h / 0 °C

1.2: 1 h

2.1: water; lithium hydroxide / tetrahydrofuran / 20 °C

3.1: caesium carbonate / N,N-dimethyl-formamide / 20 °C

4.1: triethylamine; methanesulfonyl chloride / dichloromethane / 0 - 20 °C

5.1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 17 h / 90 °C

6.1: palladium 10% on activated carbon; hydrogen / tetrahydrofuran / 3102.97 Torr

7.1: triethylamine; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate / N,N-dimethyl-formamide; dichloromethane

8.1: Chiral Pak OD / Resolution of racemate

With hydrogenchloride; palladium 10% on activated carbon; water; hydrogen; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; caesium carbonate; methanesulfonyl chloride; triethylamine; N-ethyl-N,N-diisopropylamine; lithium hydroxide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2013.06.027

Reference yield:

: 745019-94-7
C₁₃H₁₈O₅

: 745020-01-3
C₃₆H₃₂N₄O₇S

Guidance literature:: Multi-step reaction with 6 steps

1: caesium carbonate / N,N-dimethyl-formamide / 20 °C

2: triethylamine; methanesulfonyl chloride / dichloromethane / 0 - 20 °C

3: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 17 h / 90 °C

4: palladium 10% on activated carbon; hydrogen / tetrahydrofuran / 3102.97 Torr

5: triethylamine; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate / N,N-dimethyl-formamide; dichloromethane

6: Chiral Pak OD / Resolution of racemate

With palladium 10% on activated carbon; hydrogen; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; caesium carbonate; methanesulfonyl chloride; triethylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2013.06.027

Reference yield:

: 745019-95-8
C₂₀H₂₄O₅

: 745020-01-3
C₃₆H₃₂N₄O₇S

Guidance literature:: Multi-step reaction with 5 steps

1: triethylamine; methanesulfonyl chloride / dichloromethane / 0 - 20 °C

2: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 17 h / 90 °C

3: palladium 10% on activated carbon; hydrogen / tetrahydrofuran / 3102.97 Torr

4: triethylamine; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate / N,N-dimethyl-formamide; dichloromethane

5: Chiral Pak OD / Resolution of racemate

With palladium 10% on activated carbon; hydrogen; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; methanesulfonyl chloride; triethylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2013.06.027