Boc-GlyψPhe-OH

Base Information

• Chemical Name: Boc-GlyψPhe-OH
• CAS No.: 117088-22-9
• Molecular Formula: C₁₆H₂₃NO₄S
• Molecular Weight: 325.429

Synonyms:

Chemical Property of Boc-GlyψPhe-OH

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of Boc-GlyψPhe-OH

There total 2 articles about Boc-GlyψPhe-OH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(S)-(alpha)-bromobenzenepropanoic acid (42990-55-6,35016-63-8,42990-49-8,16503-53-0) → Boc-GlyψPhe-OH (117088-22-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 51 percent / 0.5M aqueous NaHCO₃ / 24 h

2: 2.27 g / 1M NaOH / butan-1-ol; H₂O / 3 h / Ambient temperature

With sodium hydroxide; sodium hydrogencarbonate; In water; butan-1-ol;

Reference yield:

di-tert-butyl dicarbonate (24424-99-5) + (S)-2-(2-aminoethylthio)-3-phenylpropionic acid (118743-72-9) → Boc-GlyψPhe-OH (117088-22-9)

Guidance literature:

With sodium hydroxide; In water; butan-1-ol; for 3h; Ambient temperature;

Reference yield:

Boc-GlyψPhe-OH (117088-22-9) → cyclo(GlyψPhe)3 (117088-20-7)

Guidance literature:

Multi-step reaction with 2 steps

2: 4.5 mg / DPPA, HOBt / dimethylformamide / 24 h / -15 °C

With diphenyl-phosphinic acid; benzotriazol-1-ol; In N,N-dimethyl-formamide;

DOI:10.1016/S0040-4020(01)86119-6

upstream raw materials:

di-tert-butyl dicarbonate

(S)-2-(2-aminoethylthio)-3-phenylpropionic acid

(S)-(alpha)-bromobenzenepropanoic acid

Downstream raw materials:

Fmoc-Tyr-D-Lys-GlyψPhe-Leu-OH

cyclo(GlyψPhe)3

H-Tyr-cycloPhe-D-Pen>

N-t-butoxycarbonylglycyl-Ψ(CH2S)-phenylalaninamide

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