9-(benzyloxy)-8-methoxy-1,4,5,6-tetrahydrobenzoquinolin-3(2H)-one

Base Information

Chemical Name:9-(benzyloxy)-8-methoxy-1,4,5,6-tetrahydrobenzoquinolin-3(2H)-one
CAS No.:127399-67-1
Molecular Formula:C₂₁H₂₁NO₃
Molecular Weight:335.403
Hs Code.:

9-(benzyloxy)-8-methoxy-1,4,5,6-tetrahydrobenzo<f>quinolin-3(2H)-one

Synonyms:

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Chemical Property of 9-(benzyloxy)-8-methoxy-1,4,5,6-tetrahydrobenzoquinolin-3(2H)-one

Chemical Property:

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Technology Process of 9-(benzyloxy)-8-methoxy-1,4,5,6-tetrahydrobenzoquinolin-3(2H)-one

There total 3 articles about 9-(benzyloxy)-8-methoxy-1,4,5,6-tetrahydrobenzoquinolin-3(2H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3199-70-0
6-(benzyloxy)-5-methoxy-1-indanone

: 127399-67-1
9-(benzyloxy)-8-methoxy-1,4,5,6-tetrahydrobenzoquinolin-3(2H)-one

Guidance literature:: Multi-step reaction with 3 steps

1: 63 percent / t-BuOK / diethyl ether / 1 h / 25 °C

2: 1.) Tl(NO₃)3, 2.) 10percent HCl / 1.) MeOH, 1 min, 2.) MeOH, 20 h

3: 1.) pyrrolidine, p-toluenesulfonic acid / 1.) benzene, reflux, 3 h, 2.) a) 80 deg C, 3 h, b) 130 deg C, 30 min

With pyrrolidine; hydrogenchloride; potassium tert-butylate; toluene-4-sulfonic acid; thallium(III) nitrate; In diethyl ether;
DOI:10.1021/jm00169a031

Reference yield:

: 127399-65-9
6-(benzyloxy)-5-methoxy-1-methyleneindan

: 127399-67-1
9-(benzyloxy)-8-methoxy-1,4,5,6-tetrahydrobenzoquinolin-3(2H)-one

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) Tl(NO₃)3, 2.) 10percent HCl / 1.) MeOH, 1 min, 2.) MeOH, 20 h

2: 1.) pyrrolidine, p-toluenesulfonic acid / 1.) benzene, reflux, 3 h, 2.) a) 80 deg C, 3 h, b) 130 deg C, 30 min

With pyrrolidine; hydrogenchloride; toluene-4-sulfonic acid; thallium(III) nitrate;
DOI:10.1021/jm00169a031

Reference yield:

: 127399-66-0
1,2,3,4-tetrahydro-7-(benzyloxy)-6-methoxy-2(1H)-naphthalenone

: 79-06-1,12624-24-7,25038-45-3,27754-57-0,33338-03-3,39387-77-4,68247-81-4,9082-06-8,79079-15-5
2-propenamide

: 127399-67-1
9-(benzyloxy)-8-methoxy-1,4,5,6-tetrahydrobenzoquinolin-3(2H)-one

Guidance literature:: With pyrrolidine; toluene-4-sulfonic acid; Yield given. Multistep reaction; 1.) benzene, reflux, 3 h, 2.) a) 80 deg C, 3 h, b) 130 deg C, 30 min;
DOI:10.1021/jm00169a031