1,2-Cyclohexanediol, 1-[(methoxymethoxy)methyl]-4-(1-methylethyl)-

Base Information

Chemical Name:1,2-Cyclohexanediol, 1-[(methoxymethoxy)methyl]-4-(1-methylethyl)-
CAS No.:139694-07-8
Molecular Formula:C12H24O4
Molecular Weight:232.32
Hs Code.:

Synonyms:

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Chemical Property of 1,2-Cyclohexanediol, 1-[(methoxymethoxy)methyl]-4-(1-methylethyl)-

Chemical Property:

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Technology Process of 1,2-Cyclohexanediol, 1-[(methoxymethoxy)methyl]-4-(1-methylethyl)-

There total 5 articles about 1,2-Cyclohexanediol, 1-[(methoxymethoxy)methyl]-4-(1-methylethyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 139694-06-7
4-isopropenyl-1-(methoxymethoxymethyl)cyclohexane-1,2-diol

: 139694-07-8
4-isopropyl-1-(methoxymethoxymethyl)cyclohexane-1,2-diol

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; under 2206.5 Torr;

Reference yield:

: 18031-40-8
(S)-(-)-perillaldehyde

: 139694-07-8
4-isopropyl-1-(methoxymethoxymethyl)cyclohexane-1,2-diol

Guidance literature:: Multi-step reaction with 5 steps

1: 52 percent / 30percent H₂O₂, 6M NaOH / methanol / 0.5 h / Ambient temperature

2: 77 percent / NaBH₄ / methanol / 0.5 h / 0 °C

3: 83 percent / diisopropylethylamine / 1) 0 deg C, 4 h, 2) r.t., 10 h

4: 86 percent / 15percent KOH / dimethylsulfoxide / 110 °C

5: 97 percent / H₂ / 10percent Pd-C / methanol / 2206.5 Torr

With potassium hydroxide; sodium hydroxide; sodium tetrahydroborate; hydrogen; dihydrogen peroxide; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In methanol; dimethyl sulfoxide;

Reference yield:

: 139694-05-6
1,2-epoxy-4-isopropenyl-1-<(methoxymethoxy)methyl>cyclohexane

: 139694-07-8
4-isopropyl-1-(methoxymethoxymethyl)cyclohexane-1,2-diol

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / 15percent KOH / dimethylsulfoxide / 110 °C

2: 97 percent / H₂ / 10percent Pd-C / methanol / 2206.5 Torr

With potassium hydroxide; hydrogen; palladium on activated charcoal; In methanol; dimethyl sulfoxide;