(1-adamantyl)diphenylarsine oxide

Base Information

• Chemical Name: (1-adamantyl)diphenylarsine oxide
• CAS No.: 83135-26-6
• Molecular Formula: C₂₂H₂₅AsO
• Molecular Weight: 380.361
• Mol file: 83135-26-6.mol

Synonyms:

Chemical Property of (1-adamantyl)diphenylarsine oxide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (1-adamantyl)diphenylarsine oxide

There total 3 articles about (1-adamantyl)diphenylarsine oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(1-adamantyl)diphenylarsine (83135-27-7) → (1-adamantyl)diphenylarsine oxide (83135-26-6)

Guidance literature:

With silica gel; In methanol;

DOI:10.1021/jo00145a010

Reference yield:

1-Adamantyl bromide (768-90-1) → (1-adamantyl)diphenylarsine oxide (83135-26-6)

Guidance literature:

Multi-step reaction with 2 steps

1: t-butyl alcohol, liq. NH₃ / 1 h / Irradiation

2: silica gel / methanol

With ammonia; silica gel; tert-butyl alcohol; In methanol;

DOI:10.1021/jo00145a010

Reference yield:

diphenylarsenide ion (14971-22-3) → (1-adamantyl)diphenylarsine oxide (83135-26-6)

Guidance literature:

Multi-step reaction with 2 steps

1: t-butyl alcohol, liq. NH₃ / 1 h / Irradiation

2: silica gel / methanol

With ammonia; silica gel; tert-butyl alcohol; In methanol;

DOI:10.1021/jo00145a010

upstream raw materials:

(1-adamantyl)diphenylarsine

1-Adamantyl bromide

diphenylarsenide ion