teretifolione B

Base Information

Chemical Name:teretifolione B
CAS No.:166376-67-6
Molecular Formula:C₂₀H₂₀O₄
Molecular Weight:324.376
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of teretifolione B

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Technology Process of teretifolione B

There total 7 articles about teretifolione B which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 9-(benzyloxy)-3-methyl-3-(4-methylpent-3-en-1-yl)-3H-benzo[f]chromene-7,10-dione

: 166376-67-6
teretifolione B

Guidance literature:: With potassium hydroxide; In ethanol; water; at 20 ℃; for 0.416667h;
DOI:10.1016/j.tet.2017.06.050

Reference yield: 43.0%

: 166270-02-6
(+/-)-3-methyl-3-(4'-methylpent-3'-enyl)-3H-naphtho<2,1-b>pyran-9,10-dione

: 166376-67-6
teretifolione B

Guidance literature:: (+/-)-3-methyl-3-(4'-methylpent-3'-enyl)-3H-naphtho<2,1-b>pyran-9,10-dione; With sodium dithionite; In water; toluene;

With potassium tert-butylate; oxygen; In tert-butyl alcohol; at 20 ℃; for 0.0833333h; Further stages.;
DOI:10.1071/CH08177

Reference yield:

: 54246-36-5
3-methyl-3-(4'-methylpent-3'enyl)-3H-naphtho<2,1-b>pyran-9-ol

: 166376-67-6
teretifolione B

Guidance literature:: Multi-step reaction with 2 steps

1: 56 percent / Fremy's salt, Adogen 464, 10percent K₂CO₃ / benzene

2: 1.) Na₂S₂O₄, 2.) t-BuO(-), O₂ / 2.) t-BuOH

With sodium dithionite; adogen 464; potassiuim nitrosodisulfonate; t-butoxide; oxygen; potassium carbonate; In benzene;
DOI:10.1021/jo00122a008