Hydroperchlorate Salt of N-tert-Butylazetidine-2-carboxylic Acid

Base Information

• Chemical Name: Hydroperchlorate Salt of N-tert-Butylazetidine-2-carboxylic Acid
• CAS No.: 77648-08-9
• Molecular Formula: C₈H₁₅NO₂*ClHO₄
• Molecular Weight: 257.671
• Mol file: 77648-08-9.mol

Synonyms:

Chemical Property of Hydroperchlorate Salt of N-tert-Butylazetidine-2-carboxylic Acid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of Hydroperchlorate Salt of N-tert-Butylazetidine-2-carboxylic Acid

There total 2 articles about Hydroperchlorate Salt of N-tert-Butylazetidine-2-carboxylic Acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

1-tert-Butyl-azetidin-2-carbonsaeure (18085-38-6,255883-03-5,255883-28-4) → Hydroperchlorate Salt of N-tert-Butylazetidine-2-carboxylic Acid (77648-08-9)

Guidance literature:

With perchloric acid; In dichloromethane; for 1h; ice-cold CH₂Cl₂;

DOI:10.1021/jo00328a001

Reference yield:

N-tert-Butyl-2-(carbo-tert-butoxy)azetidine (77647-96-2) → Hydroperchlorate Salt of N-tert-Butylazetidine-2-carboxylic Acid (77648-08-9)

Guidance literature:

With perchloric acid; trifluoroacetic acid; Yield given. Multistep reaction; 1.) CH₂Cl₂, 0 deg C, 2.) 25 deg C, 1h;

DOI:10.1021/jo00328a001

upstream raw materials:

N-tert-Butyl-2-(carbo-tert-butoxy)azetidine

1-tert-Butyl-azetidin-2-carbonsaeure

Refernces