(2S,3R)-2-((S)-2-Benzyloxycarbonylamino-3-{[bis-(4-methoxy-phenyl)-methyl]-carbamoyl}-propionylamino)-3-[(S)-1-carboxy-2-(3H-imidazol-4-yl)-ethylamino]-butyric acid

Base Information

Chemical Name:(2S,3R)-2-((S)-2-Benzyloxycarbonylamino-3-{[bis-(4-methoxy-phenyl)-methyl]-carbamoyl}-propionylamino)-3-[(S)-1-carboxy-2-(3H-imidazol-4-yl)-ethylamino]-butyric acid
CAS No.:105424-62-2
Molecular Formula:C₃₇H₄₂N₆O₁₀
Molecular Weight:730.775
Hs Code.:

(2S,3R)-2-((S)-2-Benzyloxycarbonylamino-3-{[bis-(4-methoxy-phenyl)-methyl]-carbamoyl}-propionylamino)-3-[(S)-1-carboxy-2-(3H-imidazol-4-yl)-ethylamino]-butyric acid

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Chemical Property of (2S,3R)-2-((S)-2-Benzyloxycarbonylamino-3-{[bis-(4-methoxy-phenyl)-methyl]-carbamoyl}-propionylamino)-3-[(S)-1-carboxy-2-(3H-imidazol-4-yl)-ethylamino]-butyric acid

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of (2S,3R)-2-((S)-2-Benzyloxycarbonylamino-3-{[bis-(4-methoxy-phenyl)-methyl]-carbamoyl}-propionylamino)-3-[(S)-1-carboxy-2-(3H-imidazol-4-yl)-ethylamino]-butyric acid

There total 1 articles about (2S,3R)-2-((S)-2-Benzyloxycarbonylamino-3-{[bis-(4-methoxy-phenyl)-methyl]-carbamoyl}-propionylamino)-3-[(S)-1-carboxy-2-(3H-imidazol-4-yl)-ethylamino]-butyric acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 88495-07-2
(2S,3R)-2-amino-3-[[(1S)-1-carboxy-2-(4-imidazolyl)ethyl]amino]butyric acid

: 28252-61-1
Z-L-Asn(Mbh)OSu

: 105424-62-2,105498-65-5,105498-66-6,105498-67-7
(2S,3R)-2-((S)-2-Benzyloxycarbonylamino-3-{[bis-(4-methoxy-phenyl)-methyl]-carbamoyl}-propionylamino)-3-[(S)-1-carboxy-2-(3H-imidazol-4-yl)-ethylamino]-butyric acid

Guidance literature:: With triethylamine; In 1,4-dioxane; water; Yield given;
DOI:10.1016/S0040-4039(00)80704-2

Reference yield: 73.0%

: 105424-62-2,105498-65-5,105498-66-6,105498-67-7
(2S,3R)-2-((S)-2-Benzyloxycarbonylamino-3-{[bis-(4-methoxy-phenyl)-methyl]-carbamoyl}-propionylamino)-3-[(S)-1-carboxy-2-(3H-imidazol-4-yl)-ethylamino]-butyric acid

: 105424-59-7,105498-68-8,105498-69-9,105498-70-2
FR₉₀₀₄₉₀

Guidance literature:: With hydrogen bromide;
DOI:10.1016/S0040-4039(00)80704-2

Reference yield:

: 105424-62-2,105498-65-5,105498-66-6,105498-67-7
(2S,3R)-2-((S)-2-Benzyloxycarbonylamino-3-{[bis-(4-methoxy-phenyl)-methyl]-carbamoyl}-propionylamino)-3-[(S)-1-carboxy-2-(3H-imidazol-4-yl)-ethylamino]-butyric acid

: 88495-07-2
(2S,3R)-2-amino-3-[[(1S)-1-carboxy-2-(4-imidazolyl)ethyl]amino]butyric acid

Guidance literature:: Multi-step reaction with 2 steps

1: 73 percent / 30percent HBr

With hydrogen bromide;
DOI:10.1016/S0040-4039(00)80704-2