N-(2-methyl-5-nitrophenyl)fumaramic acid methyl ester

Base Information

Chemical Name:N-(2-methyl-5-nitrophenyl)fumaramic acid methyl ester
CAS No.:80167-62-0
Molecular Formula:C₁₂H₁₂N₂O₅
Molecular Weight:264.238
Hs Code.:

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Chemical Property of N-(2-methyl-5-nitrophenyl)fumaramic acid methyl ester

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Technology Process of N-(2-methyl-5-nitrophenyl)fumaramic acid methyl ester

There total 5 articles about N-(2-methyl-5-nitrophenyl)fumaramic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: 110-89-4
piperidine

: 72889-90-8
N-(2-methyl-5-nitrophenyl)maleamic acid methyl ester

: 80167-62-0
N-(2-methyl-5-nitrophenyl)fumaramic acid methyl ester

Guidance literature:: With acetic acid; In N,N-dimethyl-formamide; at 0 ℃; for 0.5h;
DOI:10.3891/acta.chem.scand.53-0048

Reference yield:

: 99-55-8
2-methyl-5-nitroaniline

: 80167-62-0
N-(2-methyl-5-nitrophenyl)fumaramic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / diethyl ether

2: 74 percent / sulfuric acid / 48 h / Ambient temperature

3: 20 percent / acetic acid / dimethylformamide / 0.5 h / 0 °C

With sulfuric acid; acetic acid; In diethyl ether; N,N-dimethyl-formamide;
DOI:10.3891/acta.chem.scand.53-0048

Reference yield:

: 61294-16-4
N-(2-methyl-5-nitrophenyl)maleamic acid

: 80167-62-0
N-(2-methyl-5-nitrophenyl)fumaramic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 74 percent / sulfuric acid / 48 h / Ambient temperature

2: 20 percent / acetic acid / dimethylformamide / 0.5 h / 0 °C

With sulfuric acid; acetic acid; In N,N-dimethyl-formamide;
DOI:10.3891/acta.chem.scand.53-0048