C₆₄H₄₀Br₂N₈

Base Information

Chemical Name:C₆₄H₄₀Br₂N₈
CAS No.:123489-93-0
Molecular Formula:C₆₄H₄₀Br₂N₈
Molecular Weight:1080.88
Hs Code.:

C<sub>64</sub>H<sub>40</sub>Br<sub>2</sub>N<sub>8</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₆₄H₄₀Br₂N₈

Chemical Property:

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Technology Process of C₆₄H₄₀Br₂N₈

There total 4 articles about C₆₄H₄₀Br₂N₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 123489-92-9
3,3'''-dibromo-5,5',5'',5'''-tetramethyl-1,1':3',1'':3'',1'''-quarterphenyl-2,2',2'',2'''-tetracarbonitrile

: 123489-93-0
C₆₄H₄₀Br₂N₈

Guidance literature:: With n-butyllithium; copper dichloride; Yield given. Multistep reaction; 1.) THF, hexane, -78 deg C, 10 min, 2.) -78 deg C, 15 min, then 25 deg C, 1 h;
DOI:10.1021/ja00205a016

Reference yield:

: 6968-24-7
2,6-Dibromo-4-methylaniline

: 123489-93-0
C₆₄H₄₀Br₂N₈

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) conc. sulfuric acid, NaNO₂, 2.) copper(II) sulfate, NaHCO₃ / 1.) water, acetic acid, 10 deg C - 13 deg C, 2.) benzene, 50 deg C - 55 deg C, 30 min

2: 1.) n-butyllithium, 2.) copper(II) chloride / 1.) THF, hexane, -78 deg C, 10 min, 2.) -78 deg C, 30 min

3: 1.) n-butyllithium, 2.) copper(II) chloride / 1.) THF, hexane, -78 deg C, 10 min, 2.) -78 deg C, 15 min, then 25 deg C, 2 h

4: 1.) n-butyllithium, 2.) copper(II) chloride / 1.) THF, hexane, -78 deg C, 10 min, 2.) -78 deg C, 15 min, then 25 deg C, 1 h

With n-butyllithium; sulfuric acid; sodium hydrogencarbonate; copper(II) sulfate; copper dichloride; sodium nitrite;
DOI:10.1021/ja00205a016

Reference yield:

: 59596-31-5
2,6-dibromo-4-methylbenzonitrile

: 123489-93-0
C₆₄H₄₀Br₂N₈

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) n-butyllithium, 2.) copper(II) chloride / 1.) THF, hexane, -78 deg C, 10 min, 2.) -78 deg C, 30 min

2: 1.) n-butyllithium, 2.) copper(II) chloride / 1.) THF, hexane, -78 deg C, 10 min, 2.) -78 deg C, 15 min, then 25 deg C, 2 h

3: 1.) n-butyllithium, 2.) copper(II) chloride / 1.) THF, hexane, -78 deg C, 10 min, 2.) -78 deg C, 15 min, then 25 deg C, 1 h

With n-butyllithium; copper dichloride;
DOI:10.1021/ja00205a016