Acetic acid (3aR,5S,6R,6aR)-5-[2-amino-1-(methoxy-phenyl-phosphinoyl)-ethyl]-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-yl ester; compound with acetic acid

Base Information

Chemical Name:Acetic acid (3aR,5S,6R,6aR)-5-[2-amino-1-(methoxy-phenyl-phosphinoyl)-ethyl]-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-yl ester; compound with acetic acid
CAS No.:137351-83-8
Molecular Formula:C₂H₄O₂*C₁₈H₂₆NO₇P
Molecular Weight:459.433
Hs Code.:

Acetic acid (3aR,5S,6R,6aR)-5-[2-amino-1-(methoxy-phenyl-phosphinoyl)-ethyl]-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-yl ester; compound with acetic acid

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Chemical Property of Acetic acid (3aR,5S,6R,6aR)-5-[2-amino-1-(methoxy-phenyl-phosphinoyl)-ethyl]-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-yl ester; compound with acetic acid

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Technology Process of Acetic acid (3aR,5S,6R,6aR)-5-[2-amino-1-(methoxy-phenyl-phosphinoyl)-ethyl]-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-yl ester; compound with acetic acid

There total 3 articles about Acetic acid (3aR,5S,6R,6aR)-5-[2-amino-1-(methoxy-phenyl-phosphinoyl)-ethyl]-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-yl ester; compound with acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 137012-85-2,137012-92-1,137012-93-2,137012-94-3
(5R and 5S)-3-O-acetyl-5,6-dideoxy-1,2-O-isopropylidene-5-<(R and S)-(methoxy)phenylphosphinyl>-6-nitro-α-xylo-hexofuranose

: 137351-83-8,137351-85-0,137351-87-2,137351-89-4
Acetic acid (3aR,5S,6R,6aR)-5-[2-amino-1-(methoxy-phenyl-phosphinoyl)-ethyl]-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-yl ester; compound with acetic acid

Guidance literature:: With hydrogen; acetic acid; palladium hydroxide - carbon; In ethanol; at 20 ℃; for 24h; under 760 Torr;
DOI:10.1246/bcsj.64.2398

Reference yield:

: 4969-33-9
3-O-acetyl-5,6-dideoxy-1,2-O-isopropylidene-6-C-nitro-α-D-xylo-hex-5-enofuranose

: 137351-83-8,137351-85-0,137351-87-2,137351-89-4
Acetic acid (3aR,5S,6R,6aR)-5-[2-amino-1-(methoxy-phenyl-phosphinoyl)-ethyl]-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-yl ester; compound with acetic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / triethylamine / benzene / 3 h / 25 °C

2: acetic acid, H₂ / 20percent Pd(OH)2 on carbon / ethanol / 24 h / 20 °C / 760 Torr

With hydrogen; acetic acid; triethylamine; palladium hydroxide - carbon; In ethanol; benzene;
DOI:10.1246/bcsj.64.2398

Reference yield:

: 7162-15-4,111469-75-1,121467-78-5
methyl phenylphosphinate

: 137351-83-8,137351-85-0,137351-87-2,137351-89-4
Acetic acid (3aR,5S,6R,6aR)-5-[2-amino-1-(methoxy-phenyl-phosphinoyl)-ethyl]-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-yl ester; compound with acetic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / triethylamine / benzene / 3 h / 25 °C

2: acetic acid, H₂ / 20percent Pd(OH)2 on carbon / ethanol / 24 h / 20 °C / 760 Torr

With hydrogen; acetic acid; triethylamine; palladium hydroxide - carbon; In ethanol; benzene;
DOI:10.1246/bcsj.64.2398