6,8,9,11,12,14,15,17,18,20-decahydro-6-methyl-6-<3-(phenylmethoxy)propyl><1,4>benzodioxino<2,3-c>-<1,6,9,12,15>-pentaoxacycloheptadecin

Base Information

Chemical Name:6,8,9,11,12,14,15,17,18,20-decahydro-6-methyl-6-<3-(phenylmethoxy)propyl><1,4>benzodioxino<2,3-c>-<1,6,9,12,15>-pentaoxacycloheptadecin
CAS No.:143585-63-1
Molecular Formula:C₂₉H₃₈O₈
Molecular Weight:514.616
Hs Code.:

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Chemical Property of 6,8,9,11,12,14,15,17,18,20-decahydro-6-methyl-6-<3-(phenylmethoxy)propyl><1,4>benzodioxino<2,3-c>-<1,6,9,12,15>-pentaoxacycloheptadecin

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Technology Process of 6,8,9,11,12,14,15,17,18,20-decahydro-6-methyl-6-<3-(phenylmethoxy)propyl><1,4>benzodioxino<2,3-c>-<1,6,9,12,15>-pentaoxacycloheptadecin

There total 5 articles about 6,8,9,11,12,14,15,17,18,20-decahydro-6-methyl-6-<3-(phenylmethoxy)propyl><1,4>benzodioxino<2,3-c>-<1,6,9,12,15>-pentaoxacycloheptadecin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 123845-41-0
3-methyl-3-<3-(phenylmethoxy)propyl>furo<3,4-b><1,4>benzodioxin-1-(3H)-one

: 143585-63-1
6,8,9,11,12,14,15,17,18,20-decahydro-6-methyl-6-<3-(phenylmethoxy)propyl><1,4>benzodioxino<2,3-c>-<1,6,9,12,15>-pentaoxacycloheptadecin

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / LiAlH₄ / diethyl ether / 2 h / Ambient temperature

2: 1) sodium hydride / 1) tetrahydrofuran, reflux, 2 h, 2) reflux, 36 h

With lithium aluminium tetrahydride; sodium hydride; In diethyl ether;

Reference yield:

: 13329-18-5
5-(benzyloxy)pentan-2-one

: 143585-63-1
6,8,9,11,12,14,15,17,18,20-decahydro-6-methyl-6-<3-(phenylmethoxy)propyl><1,4>benzodioxino<2,3-c>-<1,6,9,12,15>-pentaoxacycloheptadecin

Guidance literature:: Multi-step reaction with 4 steps

1: 1) diisopropylamine, n-butyllithium / 1) a) tetrahydrofuran, hexane, -5 deg C, 20 min, b) -78 deg C, 5 h, 2) THF, -78 deg C, 2 h

2: 10percent aq. HCl / dioxane / Ambient temperature

3: 91 percent / LiAlH₄ / diethyl ether / 2 h / Ambient temperature

4: 1) sodium hydride / 1) tetrahydrofuran, reflux, 2 h, 2) reflux, 36 h

With hydrogenchloride; lithium aluminium tetrahydride; n-butyllithium; sodium hydride; diisopropylamine; In 1,4-dioxane; diethyl ether;

Reference yield:

: 67471-01-6
1,4-benzodioxin-2-carboxylic acid

: 143585-63-1
6,8,9,11,12,14,15,17,18,20-decahydro-6-methyl-6-<3-(phenylmethoxy)propyl><1,4>benzodioxino<2,3-c>-<1,6,9,12,15>-pentaoxacycloheptadecin

Guidance literature:: Multi-step reaction with 4 steps

1: 1) diisopropylamine, n-butyllithium / 1) a) tetrahydrofuran, hexane, -5 deg C, 20 min, b) -78 deg C, 5 h, 2) THF, -78 deg C, 2 h

2: 10percent aq. HCl / dioxane / Ambient temperature

3: 91 percent / LiAlH₄ / diethyl ether / 2 h / Ambient temperature

4: 1) sodium hydride / 1) tetrahydrofuran, reflux, 2 h, 2) reflux, 36 h

With hydrogenchloride; lithium aluminium tetrahydride; n-butyllithium; sodium hydride; diisopropylamine; In 1,4-dioxane; diethyl ether;