N-Methyl-N-(3-nitrophenyl)-2-propene-1-sulfonamide

Base Information

Chemical Name:N-Methyl-N-(3-nitrophenyl)-2-propene-1-sulfonamide
CAS No.:310435-56-4
Molecular Formula:C₁₀H₁₂N₂O₄S
Molecular Weight:256.282
Hs Code.:
DSSTox Substance ID:DTXSID001229685
Nikkaji Number:J1.350.027D

Synonyms:DTXSID001229685;310435-56-4;N-Methyl-N-(3-nitrophenyl)-2-propene-1-sulfonamide

Suppliers and Price of N-Methyl-N-(3-nitrophenyl)-2-propene-1-sulfonamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of N-Methyl-N-(3-nitrophenyl)-2-propene-1-sulfonamide

Chemical Property:

XLogP3:1.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:4
Exact Mass:256.05177804
Heavy Atom Count:17
Complexity:382

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CN(C1=CC(=CC=C1)[N+](=O)[O-])S(=O)(=O)CC=C

Technology Process of N-Methyl-N-(3-nitrophenyl)-2-propene-1-sulfonamide

There total 2 articles about N-Methyl-N-(3-nitrophenyl)-2-propene-1-sulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 85150-02-3
prop-2-ene-1-sulfonic acid (3-nitro-phenyl)-amide

: 310435-56-4
N-methyl-N-(3-nitrophenyl)propen-3-yl sulfonamide

Guidance literature:: With potassium carbonate; potassium iodide; In N,N-dimethyl-formamide; at 20 ℃;
DOI:10.1016/S0040-4039(00)01035-2

Reference yield:

: 99-09-2
3-nitro-aniline

: 310435-56-4
N-methyl-N-(3-nitrophenyl)propen-3-yl sulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / pyridine / CH₂Cl₂ / 3 h / -20 - 20 °C

2: 90 percent / K₂CO₃ / dimethylformamide / 2 h / 20 °C

With pyridine; potassium carbonate; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)00738-4