C₄₇H₄₇⁽²⁾HN₂O₁₈

Base Information

Chemical Name:C₄₇H₄₇⁽²⁾HN₂O₁₈
CAS No.:428499-73-4
Molecular Formula:C₄₇H₄₈N₂O₁₈
Molecular Weight:929.893
Hs Code.:

C<sub>47</sub>H<sub>47</sub><sup>(2)</sup>HN<sub>2</sub>O<sub>18</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₄₇H₄₇⁽²⁾HN₂O₁₈

Chemical Property:

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Technology Process of C₄₇H₄₇⁽²⁾HN₂O₁₈

There total 10 articles about C₄₇H₄₇⁽²⁾HN₂O₁₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 87190-67-8
3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl-O-trichloroacetimidate

: 428499-70-1
C₂₇H₂₈⁽²⁾HNO₉

: 428499-73-4
C₄₇H₄₇⁽²⁾HN₂O₁₈

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; 4 A molecular sieve; In dichloromethane; at -30 ℃;
DOI:10.1016/S0008-6215(01)00295-6

Reference yield:

: 2186-92-7
p-Anisaldehyde dimethyl acetal

: 428499-73-4
C₄₇H₄₇⁽²⁾HN₂O₁₈

Guidance literature:: Multi-step reaction with 3 steps

1: camphorsulfonic acid; 4 Angstroem molecular sieves / toluene / 90 °C

2: NaBH₃CN; HCl; 4 Angstroem molecular sieves / tetrahydrofuran; diethyl ether / -30 °C

3: TMSOTf; 4 Angstroem molecular sieves / CH₂Cl₂ / -30 °C

With hydrogenchloride; trimethylsilyl trifluoromethanesulfonate; 4 A molecular sieve; camphor-10-sulfonic acid; sodium cyanoborohydride; In tetrahydrofuran; diethyl ether; dichloromethane; toluene;
DOI:10.1016/S0008-6215(01)00295-6

Reference yield:

: 129532-20-3
Acetic acid (2R,3R,4R,5S,6R)-2-allyloxy-3-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-5-hydroxy-6-hydroxymethyl-tetrahydro-pyran-4-yl ester

: 428499-73-4
C₄₇H₄₇⁽²⁾HN₂O₁₈

Guidance literature:: Multi-step reaction with 9 steps

1: 96 percent / Et₃N; imidazole / CH₂Cl₂; tetrahydrofuran

2: PPTS

3: nBu₄NF / tetrahydrofuran

4: 64 percent / (COCl)2; DMSO; Et₃N / CH₂Cl₂ / -78 - 0 °C

5: NaBD₄ / CH₂Cl₂; methanol / 0 °C

6: p-TsOH / methanol

7: camphorsulfonic acid; 4 Angstroem molecular sieves / toluene / 90 °C

8: NaBH₃CN; HCl; 4 Angstroem molecular sieves / tetrahydrofuran; diethyl ether / -30 °C

9: TMSOTf; 4 Angstroem molecular sieves / CH₂Cl₂ / -30 °C

With 1H-imidazole; hydrogenchloride; sodium borodeuteride; oxalyl dichloride; trimethylsilyl trifluoromethanesulfonate; 4 A molecular sieve; camphor-10-sulfonic acid; tetrabutyl ammonium fluoride; pyridinium p-toluenesulfonate; sodium cyanoborohydride; toluene-4-sulfonic acid; dimethyl sulfoxide; triethylamine; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; toluene; 4: Swern oxidation;
DOI:10.1016/S0008-6215(01)00295-6