B₁₀C₂H₁₁CH⁽²⁾HC₆H₁₁

Base Information

• Chemical Name: B₁₀C₂H₁₁CH⁽²⁾HC₆H₁₁
• CAS No.: 146166-00-9
• Molecular Formula: C₉H₂₄B₁₀
• Molecular Weight: 241.392
• Mol file: 146166-00-9.mol

Synonyms:

Chemical Property of B₁₀C₂H₁₁CH⁽²⁾HC₆H₁₁

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of B₁₀C₂H₁₁CH⁽²⁾HC₆H₁₁

There total 1 articles about B₁₀C₂H₁₁CH⁽²⁾HC₆H₁₁ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-o-carboranylcarbene (144466-52-4) + cyclohexane (110-82-7,25012-93-5) + Cyclohexane-d12 (1735-17-7) → B10C2H11CH(2)HC6(2)H11 (146165-99-3) + B10C2H11CH(2)HC6H11 (146166-00-9) + B10C2H11CH2C6(2)H11 (146185-18-4) + B10C2H11CH2C6H11 (146185-17-3)

Guidance literature:

In cyclohexane; Cyclohexane-d12; byproducts: 3-methyl-o-carborane; carbene (generated from irradiation of the diazo compound) reacted in 1/1 mixt. of C6H12 and C6(2)H12 (presence or absence of O2); C2B10H11CH2C6H11 and C2B10H11CH(2)HC6(2)H11 sepd. by gas chromy.), the cross cpmpounds C2B10H11CH2C6(2)H11 and C2B10H11CH(2)HC6H11 could not isolated, identified by mass spectrometry;

DOI:10.1021/ja00055a007

upstream raw materials:

3-o-carboranylcarbene

cyclohexane

Cyclohexane-d12