{(CO)5W}PH₂{N(C₆H₁₁)2}

Base Information

Chemical Name:{(CO)5W}PH₂{N(C₆H₁₁)2}
CAS No.:93492-98-9
Molecular Formula:C₁₇H₂₄NO₅PW
Molecular Weight:537.205
Hs Code.:

{(CO)5W}PH<sub>2</sub>{N(C<sub>6</sub>H<sub>11</sub>)2}

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of {(CO)5W}PH₂{N(C₆H₁₁)2}

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Technology Process of {(CO)5W}PH₂{N(C₆H₁₁)2}

There total 1 articles about {(CO)5W}PH₂{N(C₆H₁₁)2} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 34.0%

: 14040-11-0
tungsten hexacarbonyl

: 93583-23-4
(dicyclohexylamino)phosphine

: 93492-98-9
{(CO)5W}PH₂{N(C₆H₁₁)2}

Guidance literature:: With tetrahydrofuran; In tetrahydrofuran; Irradiation (UV/VIS); prepn. of (THF)W(CO)5 by overnight UV-irradiation of W(CO)6 in THF, stirring at room temp. for 48 h with the phosphine;

Reference yield: 60.0%

: 93492-98-9
{(CO)5W}PH₂{N(C₆H₁₁)2}

: 107-06-2,52399-93-6
1,2-dichloro-ethane

: 137142-27-9
{(CO)5W}P(C₂H₄){N(C₆H₁₁)2}

Guidance literature:: With n-butyl lithium; In tetrahydrofuran; hexane; to THF soln. of W-complex and are added 2 equiv. of n-BuLi in n-hexane at -78°C, addn. of ClCH2CH2Cl, soln. kept at -78°C for 1h, then allowed to warm to room temp.;
DOI:10.1039/c39910001305

Reference yield:

: 93492-98-9
{(CO)5W}PH₂{N(C₆H₁₁)2}

: {(CO)5W}{N(C₆H₁₁)2}PP{CC(CH₃)3}(C₆Cl₄O₂)2

Guidance literature:: Multi-step reaction with 2 steps

1: n-butyl lithium / tetrahydrofuran; hexane

2: dichloromethane

With n-butyl lithium; In tetrahydrofuran; hexane; dichloromethane;
DOI:10.1039/c39910001305