mer-ReCl₃(2,4,6-trimethylphenyl isocyanide)3

Base Information

• Chemical Name: mer-ReCl₃(2,4,6-trimethylphenyl isocyanide)3
• CAS No.: 87829-95-6
• Molecular Formula: C₃₀H₃₃Cl₃N₃Re
• Molecular Weight: 728.178

Synonyms:

Chemical Property of mer-ReCl₃(2,4,6-trimethylphenyl isocyanide)3

Chemical Property:

Purity/Quality:

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Technology Process of mer-ReCl₃(2,4,6-trimethylphenyl isocyanide)3

There total 1 articles about mer-ReCl₃(2,4,6-trimethylphenyl isocyanide)3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 27.0%

(n-Bu4N)2Re2Cl8 + 2-mesityl isocyanide (57116-96-8) → [Re(2,4,6-trimethylphenyl isocyanide)6][trans-ReCl4(2,4,6-trimethylphenyl isocyanide)2] (87829-94-5) + mer-ReCl3(2,4,6-trimethylphenyl isocyanide)3 (87829-95-6)

Guidance literature:

In methanol; (N2); complex soln. treated with ligand, stirred for 4 h at room temp.; pptd. at 0°C, filtered, washed with cold MeOH, petroleum ether; elem. anal.;

DOI:10.1021/om00080a014

Reference yield:

mer-ReCl3(2,4,6-trimethylphenyl isocyanide)3 (87829-95-6) + 2-mesityl isocyanide (57116-96-8) → [Re(2,4,6-trimethylphenyl isocyanide)6](1+) (87829-91-2)

Guidance literature:

With potassium hexafluorophosphate; In methanol; (N2); Re complex refluxed for 12 h in MeOH contg. ligand, evapd. under N2 stream, treated with KPF6 soln. in acetone, stirred in air for 1 h; evapd., extd. (CH2Cl2), evapd., not isolated, detected by cyclic voltammetry;

DOI:10.1021/om00080a014

upstream raw materials:

2-mesityl isocyanide

Downstream raw materials:

[Re(2,4,6-trimethylphenyl isocyanide)6]⁽¹⁺⁾

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