trans-dichlorobis[(1-cyclohexenyl)diphenylphosphine]platinum(II)

Base Information

Chemical Name:trans-dichlorobis[(1-cyclohexenyl)diphenylphosphine]platinum(II)
CAS No.:332924-96-6
Molecular Formula:C₃₆H₃₈Cl₂P₂Pt
Molecular Weight:798.631
Hs Code.:

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Chemical Property of trans-dichlorobis[(1-cyclohexenyl)diphenylphosphine]platinum(II)

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Technology Process of trans-dichlorobis[(1-cyclohexenyl)diphenylphosphine]platinum(II)

There total 3 articles about trans-dichlorobis[(1-cyclohexenyl)diphenylphosphine]platinum(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 183293-92-7,183506-91-4,1209494-94-9
cis-(methyl p-tolyl sulfoxide pyridine platinum(II) chloride complex)

: 82201-23-8
(1-cyclohexenyl)diphenylphosphine

: 332924-96-6,332402-19-4
trans-dichlorobis[(1-cyclohexenyl)diphenylphosphine]platinum(II)

Guidance literature:: In dichloromethane; Pt complex added with stirring under Ar to a soln. of the ligand; refluxed for 0.5 h; cooled, the product pptd. with hexane, filtered off, washed with large volume of EtOH and dry Et2O, dried in vacuo; identified by elem. anal.;

Reference yield: 75.0%

: 75992-73-3,25794-47-2,30729-25-0,15274-33-6,22840-91-1,14568-13-9
cis-dichlorobis(dimethylsulfoxide)platinum(II)

: 82201-23-8
(1-cyclohexenyl)diphenylphosphine

: 332924-96-6,332402-19-4
cis-dichlorobis[(1-cyclohexenyl)diphenylphosphine]platinum(II)

Guidance literature:: In dichloromethane; Pt complex added with stirring under Ar to a soln. of the excess of a ligand; refluxed for 0.5 h; cooled, the product pptd. with hexane, filtered off, washed with large volume of EtOH and dry Et2O, dried in vacuo; identified by elem. anal.;

Reference yield: 50.0%

: 75992-73-3,25794-47-2,30729-25-0,15274-33-6,22840-91-1,14568-13-9
cis-dichlorobis(dimethylsulfoxide)platinum(II)

: 82201-23-8
(1-cyclohexenyl)diphenylphosphine

: 332924-96-6,332402-19-4
trans-dichlorobis[(1-cyclohexenyl)diphenylphosphine]platinum(II)

Guidance literature:: In chloroform; an excess of Pt complex added with stirring under Ar to a soln. of the ligand; refluxed for 0.5 h; cooled, the product pptd. with hexane, filtered off, washed with large volume of EtOH and dry Et2O, dried in vacuo; identified by elem. anal.;