[(2,4-di-tert-butyl-6-(bis(3,5-dimethylpyrazol-1-yl)methyl)phenol-H)AlMe][MeB(C₆F₅)3]

Base Information

• Chemical Name: [(2,4-di-tert-butyl-6-(bis(3,5-dimethylpyrazol-1-yl)methyl)phenol-H)AlMe][MeB(C₆F₅)3]
• CAS No.: 873815-52-2
• Molecular Formula: C₁₉H₃BF₁₅*C₂₆H₃₈AlN₄O
• Molecular Weight: 976.615

Synonyms:

Chemical Property of [(2,4-di-tert-butyl-6-(bis(3,5-dimethylpyrazol-1-yl)methyl)phenol-H)AlMe][MeB(C₆F₅)3]

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Technology Process of [(2,4-di-tert-butyl-6-(bis(3,5-dimethylpyrazol-1-yl)methyl)phenol-H)AlMe][MeB(C₆F₅)3]

There total 2 articles about [(2,4-di-tert-butyl-6-(bis(3,5-dimethylpyrazol-1-yl)methyl)phenol-H)AlMe][MeB(C₆F₅)3] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

[(2,4-di-tert-butyl-6-(bis(3,5-dimethylpyrazol-1-yl)methyl)phenol-H)AlMe2]*1/2C7H8 + tris(pentafluorophenyl)borate (1109-15-5) → [(2,4-di-tert-butyl-6-(bis(3,5-dimethylpyrazol-1-yl)methyl)phenol-H)AlMe][MeB(C6F5)3] (873815-52-2)

Guidance literature:

In dichloromethane; (N2 atm.; Schlenk) complex and B(C6F5)3 were dissolved in CH2Cl2, stirred for 30 min at room temp.; evapd. to dryness, triturated with cold hexane, filtered off, the solid residue was dried under vac.; elem. anal.;

DOI:10.1021/om050902e

Reference yield:

(3,5-di-tert-butyl-2-hydroxyphenyl)bis(3,5-dimethyl-pyrazolyl)methane (615553-86-1) → [(2,4-di-tert-butyl-6-(bis(3,5-dimethylpyrazol-1-yl)methyl)phenol-H)AlMe][MeB(C6F5)3] (873815-52-2)

Guidance literature:

Multi-step reaction with 2 steps

1: hexane

2: dichloromethane

In hexane; dichloromethane;

DOI:10.1021/om050902e

Reference yield:

hexahydro-2H-oxepin-2-one (502-44-3,24980-41-4,80137-66-2) + [(2,4-di-tert-butyl-6-(bis(3,5-dimethylpyrazol-1-yl)methyl)phenol-H)AlMe][MeB(C6F5)3] (873815-52-2) → [(2,4-di-tert-butyl-6-(bis(3,5-dimethylpyrazol-1-yl)methyl)phenyl 6-hydroxyhexanoate)AlMe][MeB(C6F5)3]

Guidance literature:

In benzene-d6; (N2 atm.; Schlenk) a soln. of caprolactone in C6D6 was added to a soln. of complex in C6D6 in NMR tube, the soln. was heated at 50°C for 24 h; detected by NMR spectra;

DOI:10.1021/om050902e

upstream raw materials:

tris(pentafluorophenyl)borate

(3,5-di-tert-butyl-2-hydroxyphenyl)bis(3,5-dimethyl-pyrazolyl)methane

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