1,4-benzenedicarboxylic acid-d2

Base Information

• Chemical Name: 1,4-benzenedicarboxylic acid-d2
• CAS No.: 4123-70-0
• Molecular Formula: C₈H₆O₄
• Molecular Weight: 168.117

Synonyms:

Chemical Property of 1,4-benzenedicarboxylic acid-d2

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of 1,4-benzenedicarboxylic acid-d2

There total 1 articles about 1,4-benzenedicarboxylic acid-d2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

terephthalic acid (100-21-0) → 1,4-benzenedicarboxylic acid-d2 (4123-70-0)

Guidance literature:

With water-d2; In tetrahydrofuran; Heating;

DOI:10.1016/j.saa.2014.03.125

Reference yield:

1,4-benzenedicarboxylic acid-d2 (4123-70-0) + silver nitrate + zinc(II) chloride (7646-85-7,24359-56-6) → Zn4O(1,4-benzenedicarboxylate)3

Guidance literature:

With N-ethylpropionamide; In further solvent(s); byproducts: AgCl, CO2, D2; High Pressure; (Ar); water-free soln. of Zn(NO3)2 in diethylformamide prepared by dissolving ZnCl2 and AgNO3; AgCl filtered off; 1,4-benzenedicarboxylic acid-d2 and D2O added; placed in an autoclave; purged with argon; heated and kept at 105°C for 20-24 h; further byproducts: HD, H2, HCOOD, N2O, H2O, Et2NH, Et2NNO;

DOI:10.1021/jp0708291

upstream raw materials:

terephthalic acid

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