2,2',2'',2'''-{{(2S)-3-{{4'-{[2-acetamido-4-O-(2-acetamido-2-deoxy-β-D-glucopyranosyl)-2-deoxy-β-D-glucopyranosyl]carbamoyl}biphenyl-4-yl}amino}-3-oxopropane-1,2-diyl}dinitrilo}tetraacetic acid

Base Information

Chemical Name:2,2',2'',2'''-{{(2S)-3-{{4'-{[2-acetamido-4-O-(2-acetamido-2-deoxy-β-D-glucopyranosyl)-2-deoxy-β-D-glucopyranosyl]carbamoyl}biphenyl-4-yl}amino}-3-oxopropane-1,2-diyl}dinitrilo}tetraacetic acid
CAS No.:1314582-97-2
Molecular Formula:C₄₀H₅₂N₆O₂₀
Molecular Weight:936.881
Hs Code.:

2,2',2'',2'''-{{(2S)-3-{{4'-{[2-acetamido-4-O-(2-acetamido-2-deoxy-β-D-glucopyranosyl)-2-deoxy-β-D-glucopyranosyl]carbamoyl}biphenyl-4-yl}amino}-3-oxopropane-1,2-diyl}dinitrilo}tetraacetic acid

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Chemical Property of 2,2',2'',2'''-{{(2S)-3-{{4'-{[2-acetamido-4-O-(2-acetamido-2-deoxy-β-D-glucopyranosyl)-2-deoxy-β-D-glucopyranosyl]carbamoyl}biphenyl-4-yl}amino}-3-oxopropane-1,2-diyl}dinitrilo}tetraacetic acid

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Technology Process of 2,2',2'',2'''-{{(2S)-3-{{4'-{[2-acetamido-4-O-(2-acetamido-2-deoxy-β-D-glucopyranosyl)-2-deoxy-β-D-glucopyranosyl]carbamoyl}biphenyl-4-yl}amino}-3-oxopropane-1,2-diyl}dinitrilo}tetraacetic acid

There total 10 articles about 2,2',2'',2'''-{{(2S)-3-{{4'-{[2-acetamido-4-O-(2-acetamido-2-deoxy-β-D-glucopyranosyl)-2-deoxy-β-D-glucopyranosyl]carbamoyl}biphenyl-4-yl}amino}-3-oxopropane-1,2-diyl}dinitrilo}tetraacetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 1314582-99-4
tetra(tert-butyl) 2,2',2'',2'''-{{(2S)-3-{{4'-{[2-acetamido-4-O-(2-acetamido-2-deoxy-β-D-glucopyranosyl)-2-deoxy-β-D-glucopyranosyl]carbamoyl}biphenyl-4-yl}amino}-3-oxopropane-1,2-diyl}dinitrilo}tetraacetate

: 1314582-97-2
2,2',2'',2'''-{{(2S)-3-{{4'-{[2-acetamido-4-O-(2-acetamido-2-deoxy-β-D-glucopyranosyl)-2-deoxy-β-D-glucopyranosyl]carbamoyl}biphenyl-4-yl}amino}-3-oxopropane-1,2-diyl}dinitrilo}tetraacetic acid

Guidance literature:: With chlorotriisopropylsilane; trifluoroacetic acid; In dichloromethane; for 24h;
DOI:10.1039/c1cc11860a

Reference yield:

: (S)-2,3-bis[di(tert-butoxycarbonylmethyl)amino]propionic acid

: 1314582-97-2
2,2',2'',2'''-{{(2S)-3-{{4'-{[2-acetamido-4-O-(2-acetamido-2-deoxy-β-D-glucopyranosyl)-2-deoxy-β-D-glucopyranosyl]carbamoyl}biphenyl-4-yl}amino}-3-oxopropane-1,2-diyl}dinitrilo}tetraacetic acid

Guidance literature:: Multi-step reaction with 4 steps

1: N-ethyl-N,N-diisopropylamine; HATU / dichloromethane; dimethyl sulfoxide / 24 h / 20 °C

2: tetrabutyl ammonium fluoride / tetrahydrofuran; N,N-dimethyl-formamide / 24 h

3: N-ethyl-N,N-diisopropylamine; HATU / dichloromethane; dimethyl sulfoxide / 24 h

4: chlorotriisopropylsilane; trifluoroacetic acid / dichloromethane / 24 h

With chlorotriisopropylsilane; tetrabutyl ammonium fluoride; N-ethyl-N,N-diisopropylamine; HATU; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1039/c1cc11860a

Reference yield:

: 1314582-95-0
2-(trimethylsilyl)ethyl 4'-aminobiphenyl-4-carboxylate

: 1314582-97-2
2,2',2'',2'''-{{(2S)-3-{{4'-{[2-acetamido-4-O-(2-acetamido-2-deoxy-β-D-glucopyranosyl)-2-deoxy-β-D-glucopyranosyl]carbamoyl}biphenyl-4-yl}amino}-3-oxopropane-1,2-diyl}dinitrilo}tetraacetic acid

Guidance literature:: Multi-step reaction with 4 steps

1: N-ethyl-N,N-diisopropylamine; HATU / dichloromethane; dimethyl sulfoxide / 24 h / 20 °C

2: tetrabutyl ammonium fluoride / tetrahydrofuran; N,N-dimethyl-formamide / 24 h

3: N-ethyl-N,N-diisopropylamine; HATU / dichloromethane; dimethyl sulfoxide / 24 h

4: chlorotriisopropylsilane; trifluoroacetic acid / dichloromethane / 24 h

With chlorotriisopropylsilane; tetrabutyl ammonium fluoride; N-ethyl-N,N-diisopropylamine; HATU; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1039/c1cc11860a