C₆₀H₆₀N₄O₁₂

Base Information

• Chemical Name: C₆₀H₆₀N₄O₁₂
• CAS No.: 1123264-80-1
• Molecular Formula: C₆₀H₆₀N₄O₁₂
• Molecular Weight: 1029.16
• Mol file: 1123264-80-1.mol

Synonyms:

Chemical Property of C₆₀H₆₀N₄O₁₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₆₀H₆₀N₄O₁₂

There total 2 articles about C₆₀H₆₀N₄O₁₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

meso-tetramethyltetrakis(3-hydroxyphenyl)calix[4]pyrrole (257948-49-5) + bromoacetic acid methyl ester (96-32-2) → C60H60N4O12 (1123264-80-1)

Guidance literature:

meso-tetramethyltetrakis(3-hydroxyphenyl)calix[4]pyrrole; With potassium carbonate; In acetone; for 2h;

bromoacetic acid methyl ester; In acetone; for 120h; Reflux;

DOI:10.1021/ja305684m

Reference yield:

bromoacetic acid methyl ester (96-32-2) + α,α,α,α-meso-tetramethyl-meso-tetra-4-hydroxyphenylcalix[4]pyrrole (255389-22-1) → C60H60N4O12 (1123264-80-1)

Guidance literature:

α,α,α,α-meso-tetramethyl-meso-tetra-4-hydroxyphenylcalix[4]pyrrole; With potassium carbonate; In acetone; for 2h;

bromoacetic acid methyl ester; In acetone; for 5h; Reflux;

Reference yield:

4-Phenylpyridine 1-oxide (1131-61-9) + C60H60N4O12 (1123264-80-1) → C11H9NO*C60H60N4O12 (1123264-92-5)

Guidance literature:

In [D₃]acetonitrile; at 24.84 ℃;

upstream raw materials:

bromoacetic acid methyl ester

α,α,α,α-meso-tetramethyl-meso-tetra-4-hydroxyphenylcalix[4]pyrrole

meso-tetramethyltetrakis(3-hydroxyphenyl)calix[4]pyrrole

Downstream raw materials:

C₅H₅NO*C₆₀H₆₀N₄O₁₂

C₁₁H₉NO*C₆₀H₆₀N₄O₁₂