C₄₈H₇₇NO₂

Base Information

Chemical Name:C₄₈H₇₇NO₂
CAS No.:1357168-97-8
Molecular Formula:C₄₈H₇₇NO₂
Molecular Weight:700.145
Hs Code.:

C<sub>48</sub>H<sub>77</sub>NO<sub>2</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₄₈H₇₇NO₂

Chemical Property:

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Technology Process of C₄₈H₇₇NO₂

There total 3 articles about C₄₈H₇₇NO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1357168-95-6
3,4-di(4-hexadecylphenyl)-1-tosylpyrrole

: 1357168-97-8
C₄₈H₇₇NO₂

Guidance literature:: With potassium hydroxide; In tetrahydrofuran; dichloromethane; at 20 ℃; for 42h; Inert atmosphere;
DOI:10.1039/c2cc17282h

Reference yield:

: 1206159-46-7
2-(4-hexadecyloxyphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 1357168-97-8
C₄₈H₇₇NO₂

Guidance literature:: Multi-step reaction with 2 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; caesium carbonate / 1,2-dimethoxyethane / 24 h / 20 °C / Inert atmosphere; Reflux

2: potassium hydroxide / tetrahydrofuran; dichloromethane / 42 h / 20 °C / Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; caesium carbonate; potassium hydroxide; In tetrahydrofuran; 1,2-dimethoxyethane; dichloromethane;
DOI:10.1039/c2cc17282h

Reference yield:

: 30752-21-7
1-bromo-4-(hexadecyloxy)benzene

: 1357168-97-8
C₄₈H₇₇NO₂

Guidance literature:: Multi-step reaction with 3 steps

1: bis-triphenylphosphine-palladium(II) chloride; potassium acetate / 24 h / 100 °C / Inert atmosphere

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; caesium carbonate / 1,2-dimethoxyethane / 24 h / 20 °C / Inert atmosphere; Reflux

3: potassium hydroxide / tetrahydrofuran; dichloromethane / 42 h / 20 °C / Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium acetate; caesium carbonate; potassium hydroxide; In tetrahydrofuran; 1,2-dimethoxyethane; dichloromethane;
DOI:10.1039/c2cc17282h