Technology Process of C15H18N2O3S*C2HF3O2
There total 6 articles about C15H18N2O3S*C2HF3O2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sodium hydride / mineral oil; tetrahydrofuran / 0.25 h / Inert atmosphere
1.2: 2.5 h / Inert atmosphere
2.1: (S)-1-methyl-3,3-diphenyl-hexahydropyrrolo[1,2-c][1,3,2]oxazaborole; dimethyl sulfide borane / tetrahydrofuran / 3 h / 0 - 20 °C / Inert atmosphere
3.1: dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere
With
dimethyl sulfide borane; sodium hydride; (S)-1-methyl-3,3-diphenyl-hexahydropyrrolo[1,2-c][1,3,2]oxazaborole;
In
tetrahydrofuran; dichloromethane; mineral oil;
DOI:10.1039/c3ob27111k
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sodium hydride / mineral oil; tetrahydrofuran / 0.25 h / Inert atmosphere
1.2: 2.5 h / Inert atmosphere
2.1: (S)-1-methyl-3,3-diphenyl-hexahydropyrrolo[1,2-c][1,3,2]oxazaborole; dimethyl sulfide borane / tetrahydrofuran / 3 h / 0 - 20 °C / Inert atmosphere
3.1: dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere
With
dimethyl sulfide borane; sodium hydride; (S)-1-methyl-3,3-diphenyl-hexahydropyrrolo[1,2-c][1,3,2]oxazaborole;
In
tetrahydrofuran; dichloromethane; mineral oil;
DOI:10.1039/c3ob27111k
- Guidance literature:
-
Multi-step reaction with 2 steps
1: (S)-1-methyl-3,3-diphenyl-hexahydropyrrolo[1,2-c][1,3,2]oxazaborole; dimethyl sulfide borane / tetrahydrofuran / 3 h / 0 - 20 °C / Inert atmosphere
2: dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere
With
dimethyl sulfide borane; (S)-1-methyl-3,3-diphenyl-hexahydropyrrolo[1,2-c][1,3,2]oxazaborole;
In
tetrahydrofuran; dichloromethane;
DOI:10.1039/c3ob27111k